1-cyclooctyl-2-propynyl pentafluorobenzoate

Base Information

Chemical Name:1-cyclooctyl-2-propynyl pentafluorobenzoate
CAS No.:1291103-57-5
Molecular Formula:C₁₈H₁₇F₅O₂
Molecular Weight:360.324
Hs Code.:

Synonyms:1-cyclooctyl-2-propynyl pentafluorobenzoate

Suppliers and Price of 1-cyclooctyl-2-propynyl pentafluorobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-cyclooctyl-2-propynyl pentafluorobenzoate

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Technology Process of 1-cyclooctyl-2-propynyl pentafluorobenzoate

There total 2 articles about 1-cyclooctyl-2-propynyl pentafluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: C₁₁H₁₈O

: 1291103-57-5
1-cyclooctyl-2-propynyl pentafluorobenzoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol200703g

Reference yield:

: 6688-11-5
cyclooctylcarboxaldehyde

: 1291103-57-5
1-cyclooctyl-2-propynyl pentafluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ol200703g

Reference yield:

: 1291103-57-5
1-cyclooctyl-2-propynyl pentafluorobenzoate

: 100-61-8
N-methylaniline

: N-(1-cyclooctyl-2-propynyl)-N-methylaniline

: 1291103-71-3
N-(1-cyclooctyl-2-propynyl)-N-methylaniline

Guidance literature:: With R-(+)-1,1'-binaphthyl-2,2'-diphenylphosphine; copper(I) triflate benzene complex; N-ethyl-N,N-diisopropylamine; In methanol; at 0 ℃; for 96h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol200703g