N(α)-[2-(trans-2-hexenyl)amino-4,5-dimethoxy]benzoyl-L-leucinyl-D-glutamine

Base Information

Chemical Name:N(α)-[2-(trans-2-hexenyl)amino-4,5-dimethoxy]benzoyl-L-leucinyl-D-glutamine
CAS No.:1003940-98-4
Molecular Formula:C₂₆H₄₀N₄O₇
Molecular Weight:520.626
Hs Code.:

Synonyms:N(α)-[2-(trans-2-hexenyl)amino-4,5-dimethoxy]benzoyl-L-leucinyl-D-glutamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N(α)-[2-(trans-2-hexenyl)amino-4,5-dimethoxy]benzoyl-L-leucinyl-D-glutamine

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Technology Process of N(α)-[2-(trans-2-hexenyl)amino-4,5-dimethoxy]benzoyl-L-leucinyl-D-glutamine

There total 1 articles about N(α)-[2-(trans-2-hexenyl)amino-4,5-dimethoxy]benzoyl-L-leucinyl-D-glutamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.8%

: 6728-26-3
(E)-2-Hexenal

: 4998-07-6
4,5-dimethoxy-2-nitro-benzoic acid

: 35661-60-0
Fmoc-Leu-OH

: 109745-15-5
(R)-4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(tert-butoxy)-5-oxopentanoic acid

: 1003940-98-4
N(α)-[2-(trans-2-hexenyl)amino-4,5-dimethoxy]benzoyl-L-leucinyl-D-glutamine

Guidance literature:: (R)-4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(tert-butoxy)-5-oxopentanoic acid; With benzotriazol-1-ol; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 3h; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h; solid phase reaction;

(E)-2-Hexenal; 4,5-dimethoxy-2-nitro-benzoic acid; Fmoc-Leu-OH; Further stages;
DOI:10.1016/j.bmcl.2011.05.056