2,5-dimethoxyisophthalic acid methyl ester

Base Information

Chemical Name:2,5-dimethoxyisophthalic acid methyl ester
CAS No.:479065-63-9
Molecular Formula:C₁₂H₁₄O₆
Molecular Weight:254.24
Hs Code.:

Synonyms:2,5-dimethoxyisophthalic acid methyl ester

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Chemical Property of 2,5-dimethoxyisophthalic acid methyl ester

Chemical Property:

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Technology Process of 2,5-dimethoxyisophthalic acid methyl ester

There total 4 articles about 2,5-dimethoxyisophthalic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4623-82-9
2,5-Dimethoxy-1,3-benzoldicarbonitril

: 479065-63-9
2,5-dimethoxyisophthalic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / aq. NaOH; H₂O₂ / ethanol / 0.5 h / 40 °C

2: 92 percent / aq. H₂SO₄ / 5 h / 120 °C

3: SOCl₂ / 0.5 h / Heating

4: 101 mg / Et₃N / 0.08 h

With sodium hydroxide; thionyl chloride; sulfuric acid; dihydrogen peroxide; triethylamine; In ethanol;
DOI:10.1021/jm020285l

Reference yield:

: 627101-26-2
2,5-dimethoxy-isophthalic acid

: 479065-63-9
2,5-dimethoxyisophthalic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 0.5 h / Heating

2: 101 mg / Et₃N / 0.08 h

With thionyl chloride; triethylamine;
DOI:10.1021/jm020285l

Reference yield:

: 479065-62-8
1,3-dicarbamyl-2,5-dimethoxybenzene

: 479065-63-9
2,5-dimethoxyisophthalic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / aq. H₂SO₄ / 5 h / 120 °C

2: SOCl₂ / 0.5 h / Heating

3: 101 mg / Et₃N / 0.08 h

With thionyl chloride; sulfuric acid; triethylamine;
DOI:10.1021/jm020285l