4-nitrophenyl ursodeoxycholate

Base Information

• Chemical Name: 4-nitrophenyl ursodeoxycholate
• CAS No.: 91613-11-5
• Molecular Formula: C₃₀H₄₃NO₆
• Molecular Weight: 513.675

Synonyms:4-nitrophenyl ursodeoxycholate

Chemical Property of 4-nitrophenyl ursodeoxycholate

Chemical Property:

Purity/Quality:

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Technology Process of 4-nitrophenyl ursodeoxycholate

There total 1 articles about 4-nitrophenyl ursodeoxycholate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + ursodeoxycholic acid (128-13-2) → 4-nitrophenyl ursodeoxycholate (91613-11-5)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; Ambient temperature;

Reference yield: 84.7%

taurine potassium 18-crown-6 complex + 4-nitrophenyl ursodeoxycholate (91613-11-5) → tauroursodeoxycholic acid (516-35-8,13164-17-5,14605-22-2,66255-08-1,81244-85-1,81244-86-2,90082-02-3,90082-03-4,130009-03-9,132076-82-5)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

4-nitrophenyl ursodeoxycholate (91613-11-5) + Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester (3068-34-6) → (R)-4-[(3R,5R,7S,8R,9S,10S,13R,14S,17R)-3-((2R,3R,4R,5S,6R)-4,5-Diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yloxy)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentanoic acid 4-nitro-phenyl ester

Guidance literature:

With cadmium(II) carbonate; In toluene; for 8h; Heating;

DOI:10.1016/0039-128X(92)90021-Z

upstream raw materials:

4-nitro-phenol

ursodeoxycholic acid

Downstream raw materials:

tauroursodeoxycholic acid

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