4-(3,7-dimethyloctyloxy)-4'-methoxybenzil

Base Information

Chemical Name:4-(3,7-dimethyloctyloxy)-4'-methoxybenzil
CAS No.:1219732-52-1
Molecular Formula:C₂₅H₃₂O₄
Molecular Weight:396.527
Hs Code.:

Synonyms:4-(3,7-dimethyloctyloxy)-4'-methoxybenzil

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Chemical Property of 4-(3,7-dimethyloctyloxy)-4'-methoxybenzil

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Technology Process of 4-(3,7-dimethyloctyloxy)-4'-methoxybenzil

There total 1 articles about 4-(3,7-dimethyloctyloxy)-4'-methoxybenzil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 106-21-8,59204-02-3
tetrahydrogeraniol

: 54945-19-6
4-hydroxy-4'-methoxybenzil

: 1219732-52-1
4-(3,7-dimethyloctyloxy)-4'-methoxybenzil

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 2h;
DOI:10.1039/b9nj00519f

Reference yield: 53.0%

: 15857-57-5
tetraphosphorus decasulfide

: nickel(II) chloride hexahydrate

: 1219732-52-1
4-(3,7-dimethyloctyloxy)-4'-methoxybenzil

: 1219732-64-5
bis[1-(4-(3,7-dimethyloctyloxy)phenyl)-2-(4-methoxyphenyl)ethene-1,2-dithiolene]nickel

Guidance literature:: With air; In dioxane; H₂O; mixt. of dialkoxybenzil and P4S10 in dioxane heated at 130°C under reflux for 5 h, hot mixture filtered, aq. soln. of NiCl2*6H2O added tofiltrate, mixt. heated under reflux for 2 h, cooled to room temp.; small amt. of H2O added, ppt. filtered off, repeated pptn. from CH2Cl2 by addn. of EtOH, column chromy. (silica gel, hexane/CH2Cl2); elem. anal.;
DOI:10.1039/b9nj00519f