bis[1-(4-(3,7-dimethyloctyloxy)phenyl)-2-(4-methoxyphenyl)ethene-1,2-dithiolene]nickel

Base Information

Chemical Name:bis[1-(4-(3,7-dimethyloctyloxy)phenyl)-2-(4-methoxyphenyl)ethene-1,2-dithiolene]nickel
CAS No.:1219732-64-5
Molecular Formula:C₅₀H₆₄NiO₄S₄
Molecular Weight:916.01
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[1-(4-(3,7-dimethyloctyloxy)phenyl)-2-(4-methoxyphenyl)ethene-1,2-dithiolene]nickel

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Technology Process of bis[1-(4-(3,7-dimethyloctyloxy)phenyl)-2-(4-methoxyphenyl)ethene-1,2-dithiolene]nickel

There total 1 articles about bis[1-(4-(3,7-dimethyloctyloxy)phenyl)-2-(4-methoxyphenyl)ethene-1,2-dithiolene]nickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 15857-57-5
tetraphosphorus decasulfide

: nickel(II) chloride hexahydrate

: 1219732-52-1
4-(3,7-dimethyloctyloxy)-4'-methoxybenzil

: 1219732-64-5
bis[1-(4-(3,7-dimethyloctyloxy)phenyl)-2-(4-methoxyphenyl)ethene-1,2-dithiolene]nickel

Guidance literature:: With air; In dioxane; H₂O; mixt. of dialkoxybenzil and P4S10 in dioxane heated at 130°C under reflux for 5 h, hot mixture filtered, aq. soln. of NiCl2*6H2O added tofiltrate, mixt. heated under reflux for 2 h, cooled to room temp.; small amt. of H2O added, ppt. filtered off, repeated pptn. from CH2Cl2 by addn. of EtOH, column chromy. (silica gel, hexane/CH2Cl2); elem. anal.;
DOI:10.1039/b9nj00519f