Technology Process of C54H37N3O
There total 5 articles about C54H37N3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate;
In
5,5-dimethyl-1,3-cyclohexadiene;
at 120 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium phosphate; copper(l) iodide / toluene / 3 h / 120 °C
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol; water / 12 h / 120 °C
4.1: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 120 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; palladium diacetate; sodium carbonate;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol; water / 12 h / 120 °C
3.1: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 120 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; palladium diacetate; sodium carbonate;
In
tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; water; toluene;