3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide

Base Information

Chemical Name:3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide
CAS No.:212181-02-7
Molecular Formula:C₁₄H₁₈N₆O₂Si
Molecular Weight:330.421
Hs Code.:

Synonyms:3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide

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Chemical Property of 3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide

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Technology Process of 3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide

There total 5 articles about 3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 212180-85-3
3-[dimethyl(phenyl)silyl]hexanediodihydrazide

: 212181-02-7
3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; N,N-dimethyl-formamide; at -5 - 0 ℃; for 0.166667h;

Reference yield:

: 77116-74-6
(E)-2-hexenedioic acid diethyl ester

: 212181-02-7
3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / tetrahydrofuran / 3 h / -78 °C

2: KOH / ethanol / 3.5 h / Heating

3: diethyl ether

4: NH₂NH₂*H₂O / methanol / 72 h / Ambient temperature

5: NaNO₂, HCl / dimethylformamide; H₂O / 0.17 h / -5 - 0 °C

With hydrogenchloride; potassium hydroxide; hydrazine hydrate; sodium nitrite; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 3-(Dimethyl-phenyl-silanyl)-hexanedioic acid

: 212181-02-7
3-(Dimethyl-phenyl-silanyl)-hexanedioyl diazide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: NH₂NH₂*H₂O / methanol / 72 h / Ambient temperature

3: NaNO₂, HCl / dimethylformamide; H₂O / 0.17 h / -5 - 0 °C

With hydrogenchloride; hydrazine hydrate; sodium nitrite; In methanol; diethyl ether; water; N,N-dimethyl-formamide;