TRANS-2-BUTENE-1,4-DICARBOXYLIC ACID DIETHYL ESTER

Base Information

Chemical Name:TRANS-2-BUTENE-1,4-DICARBOXYLIC ACID DIETHYL ESTER
CAS No.:77116-74-6
Molecular Formula:C10H16 O4
Molecular Weight:200.235
Hs Code.:2917190090
Mol file:77116-74-6.mol

Synonyms:TRANS-3-HEXENEDIOIC ACID DIETHYL ESTER;TRANS-2-BUTENE-1,4-DICARBOXYLIC ACID DIETHYL ESTER;DIETHYL TRANS-2-BUTENE-1,4-DICARBOXYLATE;DIETHYL TRANS-BETA-DIHYDROMUCONATE

Suppliers and Price of TRANS-2-BUTENE-1,4-DICARBOXYLIC ACID DIETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of TRANS-2-BUTENE-1,4-DICARBOXYLIC ACID DIETHYL ESTER

Chemical Property:

Vapor Pressure:0.013mmHg at 25°C
Melting Point:195-196°C
Refractive Index:1.448
Boiling Point:259.4°C at 760 mmHg
Flash Point:120.2°C
PSA：52.60000
Density:1.04
LogP:1.44900

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of TRANS-2-BUTENE-1,4-DICARBOXYLIC ACID DIETHYL ESTER

There total 8 articles about TRANS-2-BUTENE-1,4-DICARBOXYLIC ACID DIETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 34780-29-5
3-oxo-propionic acid ethyl ester

: 77116-74-6
(E)-2-hexenedioic acid diethyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) r.t., 2 h, 2.) r.t., 3 h;

Reference yield: 63.0%

: 539-74-2
Ethyl 3-bromopropionate

: 82101-76-6,106335-84-6,128266-87-5
(Z)-ethyl 3-(tributylstannyl)propenoate

: 77116-74-6
(E)-2-hexenedioic acid diethyl ester

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In toluene; at 86 ℃;
DOI:10.1039/c39850000682

Reference yield:

: 64-17-5
ethanol

: 74-85-1
ethene

: 3588-17-8
trans,trans-muconic acid

: 77116-74-6
(E)-2-hexenedioic acid diethyl ester

: 72903-27-6
cyclohexane-1,4-dicarboxylic acid diethyl ester

: 636-09-9
diethyl terephthalate

Guidance literature:: ethanol; ethene; trans,trans-muconic acid; With dodecatungstosilic acid; at 200 ℃; for 6h; under 22502.3 Torr; Autoclave;

With Pd/C; at 200 ℃; for 6h; under 750.075 Torr; Autoclave; Inert atmosphere;
DOI:10.1002/anie.201509149