(5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Base Information

Chemical Name:(5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate
CAS No.:1544739-36-7
Molecular Formula:C₃₂H₃₅NO₅
Molecular Weight:513.634
Hs Code.:

(5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Synonyms:(5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

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Chemical Property of (5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

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Technology Process of (5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

There total 15 articles about (5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 822-48-0
3-chloromethyl-3-methyl oxetane

: 1544739-36-7
(5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C

2: potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine / water; 1,4-dioxane / 0.17 h / 100 °C / Inert atmosphere; Microwave irradiation

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; tricyclohexylphosphine; In 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 1458652-56-6
3-((4-bromo-3,5-dimethylphenoxy)methyl)-3-methyloxetane

: 1544739-24-3
4-[2-fluoro-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyloxy]-1,1a,6,6a-tetrahydro-3-aza-cyclopropa[a]indene-1-carboxylic acid ethyl ester

: 1544739-36-7
(5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; tricyclohexylphosphine; In 1,4-dioxane; water; at 100 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 7463-51-6
4-bromo-3,5-dimethylphenol

: 1544739-36-7
(5aR,6S,6aS)-ethyl 3-((2’,6’-dimethyl-4’-((3-methyloxetan-3-yl)methoxy)-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C

2: potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine / water; 1,4-dioxane / 0.17 h / 100 °C / Inert atmosphere; Microwave irradiation

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; tricyclohexylphosphine; In 1,4-dioxane; water; N,N-dimethyl-formamide;