Technology Process of C24H34INO9
There total 6 articles about C24H34INO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
ethyl acetate;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran; diethyl ether / 1 h / -78 °C
1.2: -78 - 20 °C
2.1: boron tribromide / dichloromethane / 0.5 h / 0 - 20 °C
3.1: potassium carbonate; potassium iodide / acetone / 12 h / Reflux
4.1: bromine / dichloromethane / 2 h / 20 °C
5.1: triethylamine / ethyl acetate / 2 h / 20 °C
With
bromine; isopropylmagnesium chloride; boron tribromide; potassium carbonate; triethylamine; potassium iodide;
In
tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron tribromide / dichloromethane / 0.5 h / 0 - 20 °C
2: potassium carbonate; potassium iodide / acetone / 12 h / Reflux
3: bromine / dichloromethane / 2 h / 20 °C
4: triethylamine / ethyl acetate / 2 h / 20 °C
With
bromine; boron tribromide; potassium carbonate; triethylamine; potassium iodide;
In
dichloromethane; ethyl acetate; acetone;