4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester

Base Information

Chemical Name:4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester
CAS No.:138824-20-1
Molecular Formula:C₃₇H₄₇F₃O₃
Molecular Weight:596.774
Hs Code.:

Synonyms:4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester

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Chemical Property of 4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester

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Technology Process of 4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester

There total 9 articles about 4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 280-57-9,88935-43-7
1,4-diaza-bicyclo[2.2.2]octane

: 4-(3-trifluoromethylheptyl)-phenol

: 60 %-sodium hydride

: 69367-32-4
4-n-decyloxy-4'-biphenylcarboxylic acid

: 138824-20-1
4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester

Guidance literature:: With thionyl chloride; In tetrahydrofuran; diethyl ether; ethanol;

Reference yield:

: 360-34-9
1,1,1-trifluoro-2-hexanone

: 138824-20-1
4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 1) NaOEt / 1) CH₂Cl₂, room temp., 2) room temp.

2: H₂ / 5percent Pd/C / methanol

3: NaOH / methanol; H₂O / Heating

4: thionyl chloride / 80 °C

5: CS₂, AlCl₃ / Heating

6: LiAlH₄, AlCl₃ / diethyl ether / Heating

7: 1) 1,4-diazabicyclo<2.2.2>octane, 2) NaH / 1) benzene, 50 deg C, 2) a) room temp., b) reflux

With 1,4-diaza-bicyclo[2.2.2]octane; carbon disulfide; sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; thionyl chloride; hydrogen; sodium ethanolate; sodium hydride; palladium on activated charcoal; In methanol; diethyl ether; water;

Reference yield:

: 121215-01-8
(Z)-3-Trifluoromethyl-hept-2-enoic acid ethyl ester

: 138824-20-1
4-decyloxybiphenyl-4'-carboxylic acid-4''(3-trifluoromethylheptyl)phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / 5percent Pd/C / methanol

2: NaOH / methanol; H₂O / Heating

3: thionyl chloride / 80 °C

4: CS₂, AlCl₃ / Heating

5: LiAlH₄, AlCl₃ / diethyl ether / Heating

6: 1) 1,4-diazabicyclo<2.2.2>octane, 2) NaH / 1) benzene, 50 deg C, 2) a) room temp., b) reflux

With 1,4-diaza-bicyclo[2.2.2]octane; carbon disulfide; sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; thionyl chloride; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; diethyl ether; water;