Technology Process of (E,E,E)-2,4,6-trimethylocta-2,4,6-trienyl(triphenyl)phosphonium bromide
There total 6 articles about (E,E,E)-2,4,6-trimethylocta-2,4,6-trienyl(triphenyl)phosphonium bromide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
methanol;
at 25 ℃;
for 144h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 73 percent / CH2Cl2 / 48 h / Heating
2: 85 percent / LiAlH4 / diethyl ether / 12 h / Heating
3: 68 percent / manganese dioxide / CH2Cl2 / Ambient temperature
4: 40 percent / CH2Cl2 / 48 h / Heating
5: 82 percent / LiAlH4 / diethyl ether / 12 h / Heating
6: 100 percent / methanol / 144 h / 25 °C
With
manganese(IV) oxide; lithium aluminium tetrahydride;
In
methanol; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 40 percent / CH2Cl2 / 48 h / Heating
2: 82 percent / LiAlH4 / diethyl ether / 12 h / Heating
3: 100 percent / methanol / 144 h / 25 °C
With
lithium aluminium tetrahydride;
In
methanol; diethyl ether; dichloromethane;