1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione

Base Information

• Chemical Name: 1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione
• CAS No.: 1039630-17-5
• Molecular Formula: C₁₇H₁₆ClN₅O₂S
• Molecular Weight: 389.865

Synonyms:1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione

Chemical Property of 1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione

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Technology Process of 1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione

There total 1 articles about 1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

2-benzylmercapto-1-(2-methoxy-5-chlorophenyl)-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione (1039630-12-0) → 1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione (1039630-17-5)

Guidance literature:

With hydrazine hydrate; In benzene; at 40 - 50 ℃; for 10h;

DOI:10.1002/jhet.5570450317

Reference yield: 55.0%

1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione (1039630-17-5) + 2-tolyl isothiocyanate (614-69-7) → N-[2-methylphenyl]-N-1-[(2-methoxy-5-chlorophenyl)-4-(4-methoxyphenyl)]-6-thioxo-1,6-dihydro-1,3,5-triazinylthiosemicarbazide (1039630-21-1)

Guidance literature:

for 0.75h; Heating;

DOI:10.1002/jhet.5570450317

Reference yield: 52.0%

1-(2-methoxy-5-chlorophenyl)-2-hydrazino-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione (1039630-17-5) + benzaldehyde (100-52-7) → N-[1-(2-methoxy-5-chlorophenyl)]-4-[(4-methoxyphenyl)-6-thioxo-1,6-dihydro-1,3,5-triazin-2-yl]-N'-benzylidene hydrazine (1039630-25-5)

Guidance literature:

With acetic acid; In ethanol; for 8h; Heating;

DOI:10.1002/jhet.5570450317

upstream raw materials:

2-benzylmercapto-1-(2-methoxy-5-chlorophenyl)-4-(4-methoxyphenyl)-1,6-dihydro-1,3,5-triazine-6-thione

Downstream raw materials:

N-[1-(2-methoxy-5-chlorophenyl)]-4-[(4-methoxyphenyl)-6-thioxo-1,6-dihydro-1,3,5-triazin-2-yl]-N'-benzylidene hydrazine

N-[2-methylphenyl]-N-1-[(2-methoxy-5-chlorophenyl)-4-(4-methoxyphenyl)]-6-thioxo-1,6-dihydro-1,3,5-triazinylthiosemicarbazide

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