(R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Base Information

Chemical Name:(R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester
CAS No.:106749-07-9
Molecular Formula:C₃₀H₅₂N₄O₄S
Molecular Weight:564.833
Hs Code.:

Synonyms:(R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

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Chemical Property of (R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

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Technology Process of (R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

There total 1 articles about (R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 106749-00-2
(S)-2-Chloro-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

: 106749-07-9
(R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 40 ℃;
DOI:10.1016/S0040-4039(00)84112-X

Reference yield:

: 106749-07-9
(R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

: 100-51-6,185532-71-2
benzyl alcohol

: (R)-2-Azido-octanoic acid benzyl ester

Guidance literature:: With titanium tetrakis(benzyl alkoxide); at 130 ℃;
DOI:10.1016/S0040-4039(00)84112-X

Reference yield:

: 106749-07-9
(R)-2-Azido-octanoic acid (1S,2R,4R)-1-[(dicyclohexylsulfamoyl)-methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

: 106819-03-8,2187-07-7
(R)-α-aminooctanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Ti(OCH₂Ph)4 / 130 °C

2: H₂ / Pd/BaSO₄ / ethanol / 760 Torr / Ambient temperature

With titanium tetrakis(benzyl alkoxide); hydrogen; Pd-BaSO₄; In ethanol;
DOI:10.1016/S0040-4039(00)84112-X