N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)

Base Information

Chemical Name:N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)
CAS No.:405885-00-9
Molecular Formula:C₃₇H₅₇Cl₂N₂O₂Yb
Molecular Weight:805.818
Hs Code.:

Synonyms:N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)

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Technology Process of N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)

There total 2 articles about N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.1%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 10361-91-8
ytterbium(III) chloride

: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-ene) lithium salt

: 405885-00-9
N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)

Guidance literature:: In tetrahydrofuran; hexane; toluene; under Ar, Schlenk techniques; soln. of ligand in toluene-hexane slowly added to suspn. of YbCl3 (molar ratio 1:1) in THF at room temp.; stirred overnight at room temp.; solvent removed under vac.; extd. with toluene; dissolved portion removed by centrifugation; filtrate concd.; cooled to -20°C; microcrystals collected by filtration; elem. anal.;
DOI:10.1021/om010803a

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 10361-91-8
ytterbium(III) chloride

: 223414-22-0
Li(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N(2,6-iPr₂C₆H₃)

: 405885-00-9
N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)

Guidance literature:: In tetrahydrofuran;
DOI:10.1016/S0022-328X(01)01478-4

Reference yield: 87.0%

: 405885-00-9
N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium dichloride bis(tetrahydrofuran)

: sodium cyclopentadienide

: 630426-38-9
N,N-2,6-diisopropylphenyl-2,4-pentanediimine ytterbium bis(cyclopentadienyl)

Guidance literature:: In tetrahydrofuran; 2 equiv. of Na compd. added to a soln. of Yb compd. at -78°C, allowed to warm to room temp., stirred for 12 h; volatiles removed (vac.), extd. (toluene), concd., kept at 4°C for 48 h, crysts. filtered; elem. anal.;
DOI:10.1021/ja050521s