phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside

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Chemical Name:phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside
CAS No.:1060735-31-0
Molecular Formula:C₂₇H₃₄O₆S₂
Molecular Weight:518.695
Hs Code.:

Synonyms:phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside

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Chemical Property of phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside

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Technology Process of phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside

There total 1 articles about phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1060735-24-1
phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 19493-09-5
Methylenetriphenylphosphorane

: 1060735-28-5
phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-6-enopyranoside

: 1060735-31-0
phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside

Guidance literature:: phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside; dimethyl sulfoxide; With oxalyl dichloride; In dichloromethane; at -75 - 45 ℃; for 1.75h;

With triethylamine; In dichloromethane; at -45 - 0 ℃; for 2.75h;

Methylenetriphenylphosphorane; In tetrahydrofuran; hexanede; at -40 - 10 ℃; for 4h;
DOI:10.1021/jo801414c