phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

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Chemical Name:phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside
CAS No.:1060735-24-1
Molecular Formula:C₂₅H₃₂O₇S
Molecular Weight:476.591
Hs Code.:

Synonyms:phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

There total 1 articles about phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 100-39-0
benzyl bromide

: 263543-42-6
phenyl 3,4-O-(2’,3’-dimethoxybutane-2’,3’-diyl)-1-thio-α-D-mannopyranoside

: 1060735-24-1
phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

: 263543-43-7
phenyl 2,6-di-O-benzyl-3,4-O-[(2S,3S)-2,3-dimethoxybutan-2,3-diyl]-1-thio-α-D-mannopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -40 - -10 ℃; for 17h;
DOI:10.1021/jo801414c

Reference yield: 84.0%

: 1060735-24-1
phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 19493-09-5
Methylenetriphenylphosphorane

: 1060735-28-5
phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-6-enopyranoside

: 1060735-31-0
phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-(E)-7-methylthio-6-enopyranoside

Guidance literature:: phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannopyranoside; dimethyl sulfoxide; With oxalyl dichloride; In dichloromethane; at -75 - 45 ℃; for 1.75h;

With triethylamine; In dichloromethane; at -45 - 0 ℃; for 2.75h;

Methylenetriphenylphosphorane; In tetrahydrofuran; hexanede; at -40 - 10 ℃; for 4h;
DOI:10.1021/jo801414c