(3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide

Base Information

Chemical Name:(3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide
CAS No.:176895-26-4
Molecular Formula:C₂₁H₂₃NO₃
Molecular Weight:337.419
Hs Code.:

Synonyms:(3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide

Chemical Property:

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Technology Process of (3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide

There total 3 articles about (3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 119-61-9
benzophenone

: 176895-25-3
(1R,3S,4R)-3,4-Dihydroxy-cyclopentanecarboxylic acid dimethylamide

: 176895-26-4
(3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 168h; Heating;

Reference yield:

: 55857-50-6
N,N-dimethylcyclopent-3-ene-1-carboxamide

: 176895-26-4
(3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / KMnO₄ / acetone / 3 h / Ambient temperature

2: 30 percent / NaOMe / propan-2-ol / 72 h / Heating

3: 11 percent / p-TsOH / toluene / 168 h / Heating

With potassium permanganate; sodium methylate; toluene-4-sulfonic acid; In isopropyl alcohol; acetone; toluene;

Reference yield:

: 176754-02-2
(1S,3R,4S)-3,4-Dihydroxy-cyclopentanecarboxylic acid dimethylamide

: 176895-26-4
(3aR,5R,6aS)-2,2-Diphenyl-tetrahydro-cyclopenta[1,3]dioxole-5-carboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / NaOMe / propan-2-ol / 72 h / Heating

2: 11 percent / p-TsOH / toluene / 168 h / Heating

With sodium methylate; toluene-4-sulfonic acid; In isopropyl alcohol; toluene;