(S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine

Base Information

Chemical Name:(S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine
CAS No.:109417-64-3
Molecular Formula:C₂₀H₂₅NO₅S
Molecular Weight:391.488
Hs Code.:

Synonyms:(S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine

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Chemical Property of (S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine

Chemical Property:

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Technology Process of (S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine

There total 5 articles about (S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-56-7
2-hydroxybromobenzene

: 109417-64-3
(S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / KI, K₂CO₃ / acetone / 90 h / Heating

2: 1.) Mg / 1.) THF, 2.) benzene, a) RT, 0.5 h, b) reflux, 3 h

3: 36 percent / Cu / methanol / Heating

4: 94 percent / 18 M aq. H₂SO₄ / 0.25 h / Ambient temperature

5: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 60 deg C, 24 h

With sulfuric acid; copper; sodium hydride; potassium carbonate; magnesium; potassium iodide; In methanol; acetone;

Reference yield:

: 109417-60-9
1-bromo-2-(2-methoxyethoxy)benzene

: 109417-64-3
(S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg / 1.) THF, 2.) benzene, a) RT, 0.5 h, b) reflux, 3 h

2: 36 percent / Cu / methanol / Heating

3: 94 percent / 18 M aq. H₂SO₄ / 0.25 h / Ambient temperature

4: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 60 deg C, 24 h

With sulfuric acid; copper; sodium hydride; magnesium; In methanol;

Reference yield:

: 109417-61-0
(S)-(-)-o-(2-methoxyethoxy)phenyl p-tolyl sulfoxide

: 109417-64-3
(S)-(+)-N-ethoxycarbonylmethyl-S-o-(2-methoxyethoxy)phenyl-S-p-tolylsulfoximine

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / Cu / methanol / Heating

2: 94 percent / 18 M aq. H₂SO₄ / 0.25 h / Ambient temperature

3: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 60 deg C, 24 h

With sulfuric acid; copper; sodium hydride; In methanol;