C₃₆H₄₇NO₄Si

Base Information

• Chemical Name: C₃₆H₄₇NO₄Si
• CAS No.: 880152-40-9
• Molecular Formula: C₃₆H₄₇NO₄Si
• Molecular Weight: 585.859
• Mol file: 880152-40-9.mol

Synonyms:C₃₆H₄₇NO₄Si

Chemical Property of C₃₆H₄₇NO₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₄₇NO₄Si

There total 19 articles about C₃₆H₄₇NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C36H45NO4Si (880152-39-6) → C36H47NO4Si (880152-40-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 48h; under 3102.89 Torr;

DOI:10.1021/ol053059p

Reference yield:

acetic acid 2-[3-amino-4-(tert-butyl-diphenyl-silanyloxy)-butyl]-cyclohex-1-enylmethyl ester (880152-28-3) → C36H47NO4Si (880152-40-9)

Guidance literature:

Multi-step reaction with 8 steps

1: 61 percent / pyridine / ethanol / 48 h / Heating

2: K₂CO₃ / methanol; H₂O / 1 h / 20 °C

3: 504.0 mg / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

4: 68 percent / Na₂SO₄; piperidinium acetate / ethyl acetate; toluene / Heating

5: 76 percent / N-chlorosuccinimide; H₂O / 2-methyl-propan-2-ol / 1 h / 20 °C

6: 66 percent / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 4 h / 20 °C

7: 98 percent / Zn; HOAc / 2 h / 20 °C

8: H₂ / 10 percent Pd/C / ethanol / 48 h / 2585.74 Torr

With pyridine; N-chloro-succinimide; tetrapropylammonium perruthennate; 4 A molecular sieve; water; hydrogen; piperdinium acetate; potassium carbonate; acetic acid; 4-methylmorpholine N-oxide; sodium sulfate; zinc; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol;

Reference yield:

4-bromo-6-butyl-2-pyrone (880152-32-9) → C36H47NO4Si (880152-40-9)

Guidance literature:

Multi-step reaction with 8 steps

1: 61 percent / pyridine / ethanol / 48 h / Heating

2: K₂CO₃ / methanol; H₂O / 1 h / 20 °C

3: 504.0 mg / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

4: 68 percent / Na₂SO₄; piperidinium acetate / ethyl acetate; toluene / Heating

5: 76 percent / N-chlorosuccinimide; H₂O / 2-methyl-propan-2-ol / 1 h / 20 °C

6: 66 percent / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 4 h / 20 °C

7: 98 percent / Zn; HOAc / 2 h / 20 °C

8: H₂ / 10 percent Pd/C / ethanol / 48 h / 2585.74 Torr

With pyridine; N-chloro-succinimide; tetrapropylammonium perruthennate; 4 A molecular sieve; water; hydrogen; piperdinium acetate; potassium carbonate; acetic acid; 4-methylmorpholine N-oxide; sodium sulfate; zinc; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol;

upstream raw materials:

C₃₆H₄₅NO₄Si

4-bromo-6-butyl-2-pyrone

2-(3-tert-butoxycarbonylamino-4-hydroxy-butyl)-cyclohex-1-enecarboxylic acid ethyl ester

4-[2-(2-ethoxycarbonyl-cyclohex-1-enyl)-ethyl]-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

Downstream raw materials:

3-(tert-butyl-diphenyl-silanyloxymethyl)-5-hexyl-2,3,8,9,10,11-hexahydro-1H,7aH-pyrrolo[2,1-j]quinolin-7-one