N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

Base Information

Chemical Name:N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine
CAS No.:163020-82-4
Molecular Formula:C₂₉H₂₈Cl₂N₆O₃
Molecular Weight:579.486
Hs Code.:

N<sup>2</sup>-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

Synonyms:N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

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Chemical Property of N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

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Technology Process of N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

There total 4 articles about N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 163020-64-2
2-(3,5-dichloroanilino)-6-chloro-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>purine

: 163020-82-4
N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

Guidance literature:: With ammonia; In methanol; at 120 ℃; for 10h;
DOI:10.1021/jm00010a026

Reference yield:

: 74564-16-2
1,3-dibenzyloxy-2-(chloromethoxy)propane

: 163020-82-4
N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 45 min, 2.) DMF, RT, 1.5 h

2: 93 percent / NH₃ / methanol / 10 h / 120 °C

With ammonia; sodium hydride; In methanol;
DOI:10.1021/jm00010a026

Reference yield:

: 163020-52-8
2-(3,5-dichloroanilino)-6-chloropurine

: 163020-82-4
N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>adenine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 45 min, 2.) DMF, RT, 1.5 h

2: 93 percent / NH₃ / methanol / 10 h / 120 °C

With ammonia; sodium hydride; In methanol;
DOI:10.1021/jm00010a026