N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide

Base Information

Chemical Name:N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide
CAS No.:1354958-39-6
Molecular Formula:C₁₇H₁₄N₆OS
Molecular Weight:350.404
Hs Code.:

Synonyms:N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide

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Technology Process of N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide

There total 4 articles about N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1354958-11-4
5-chloro-2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazoline

: 613-94-5
benzoic acid hydrazide

: 1354958-39-6
N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide

Guidance literature:: In toluene; for 2.5h; Reflux;
DOI:10.1080/00397911.2010.518780

Reference yield:

: 1354957-97-3
2-methylsulfanyl-[1,2,4]triazolo[1,5-a]quinazolin-5(4H)-one

: 1354958-39-6
N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / benzene / 2 h / Reflux

2: toluene / 2.5 h / Reflux

With trichlorophosphate; In toluene; benzene;
DOI:10.1080/00397911.2010.518780

Reference yield:

: C₁₀H₁₀N₄O₂S

: 1354958-39-6
N-(2-methylsulfanyl[1,2,4]triazolo[1,5-a]quinazolin-5-yl)benzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water / Cooling with ice; Reflux

2: trichlorophosphate / benzene / 2 h / Reflux

3: toluene / 2.5 h / Reflux

With hydrogenchloride; trichlorophosphate; In water; toluene; benzene;
DOI:10.1080/00397911.2010.518780