Technology Process of C17H23NO5
There total 5 articles about C17H23NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere
2: hydrazine hydrate / ethanol / Reflux
3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
With
di-isopropyl azodicarboxylate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran; toluene / 12 h / 0 - 20 °C
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere
3: hydrazine hydrate / ethanol / Reflux
4: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
With
di-isopropyl azodicarboxylate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane; toluene;