(4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

Base Information

Chemical Name:(4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide
CAS No.:1200122-88-8
Molecular Formula:C₂₀H₂₉NO₅
Molecular Weight:363.454
Hs Code.:

Synonyms:(4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

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Chemical Property of (4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

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Technology Process of (4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

There total 1 articles about (4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: (4-Benzyloxy)butylmagnesium bromide

: 63126-29-4,74752-95-7
(4R,5R)-2,2,N,N,N',N'-hexamethyl-1,3-dioxolane-4,5-dicarboxamide

: 1200122-88-8
(4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

: C₂₉H₃₈O₆

Guidance literature:: In tetrahydrofuran; at -15 ℃; for 0.5h;
DOI:10.1055/s-0029-1217976

Reference yield: 93.0%

: 1200122-88-8
(4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

: 1200122-89-9
(4R,5S)-5-((R)-5-(benzyloxy)-1-hydroxypentyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; at -78 ℃; for 2h; optical yield given as %de;
DOI:10.1055/s-0029-1217976

Reference yield:

: 1200122-88-8
(4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

: 1200122-89-9
(4R,5S)-5-((R)-5-(benzyloxy)-1-hydroxypentyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

: (4R,5S)-5-((S)-5-(benzyloxy)-1-hydroxypentyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide

Guidance literature:: (4R,5R)-5-(5-(benzyloxy)pentanoyl)-N,N,2,2-tetramethyl-1,3-dioxolane-4-carboxamide; With cerium(III) chloride heptahydrate; In methanol; at 20 ℃; for 1h;

With sodium tetrahydroborate; In methanol; at -78 ℃;

With water; In methanol; optical yield given as %de; stereoselective reaction;