(4R,5R)-N4,N4,N5,N5,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide

Base Information

Chemical Name:(4R,5R)-N4,N4,N5,N5,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide
CAS No.:63126-29-4
Molecular Formula:C11H20 N2 O4
Molecular Weight:244.291
Hs Code.:2932999099
DSSTox Substance ID:DTXSID40965583
Nikkaji Number:J2.418.980E
Wikidata:Q82947843
Mol file:63126-29-4.mol

Synonyms:63126-29-4;(4R,5R)-N4,N4,N5,N5,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide;(4R,5R)-4-N,4-N,5-N,5-N,2,2-hexamethyl-1,3-dioxolane-4,5-dicarboxamide;(4R,5R)-N,N,N',N'-2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide;(4R,5R)-4,5-DI(DIMETHYLAMINOCARBONYL)-2,2-DIMETHYLDIOXOLANE;5129-95-3;DTXSID40965583;AKOS024279283;[(4R,5R)-5-(N,N-dimethylcarbamoyl)-2,2-dimethyl(1,3-dioxolan-4-yl)]-N,N-dimeth ylcarboxamide;CS-0093799;(4R)-N,N,N',N',2,2-Hexamethyl-1,3-dioxolane-4beta,5alpha-biscarboxamide;(4r,5r)-N,N,N',N',2,2-hexamethyl-1,3-dioxolan-4,5-dicarboxamide;1,3-Dioxolane-4,5-dicarboxamide,n4,n4,n5,n5,2,2-hexamethyl-,(4R,5R)-;N~4~,N~4~,N~5~,N~5~,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide

Suppliers and Price of (4R,5R)-N4,N4,N5,N5,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(4R,5R)-4,5-DI(DIMETHYLAMINOCARBONYL)-2,2-DIMETHYLDIOXOLANE 95.00%
2.5G
$ 137.32

Total 11 raw suppliers

Chemical Property of (4R,5R)-N4,N4,N5,N5,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide

Chemical Property:

Melting Point:88oC
Refractive Index:1.4620 (estimate)
Boiling Point:380.6°Cat760mmHg
Flash Point:184°C
PSA：59.08000
Density:1.114g/cm³
LogP:-0.31710
XLogP3:-0.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:244.14230712
Heavy Atom Count:17
Complexity:295

Purity/Quality:

98%Min ^*data from raw suppliers

(4R,5R)-4,5-DI(DIMETHYLAMINOCARBONYL)-2,2-DIMETHYLDIOXOLANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(OC(C(O1)C(=O)N(C)C)C(=O)N(C)C)C
Isomeric SMILES:CC1(O[C@H]([C@@H](O1)C(=O)N(C)C)C(=O)N(C)C)C

Technology Process of (4R,5R)-N4,N4,N5,N5,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide

There total 4 articles about (4R,5R)-N4,N4,N5,N5,2,2-Hexamethyl-1,3-dioxolane-4,5-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 37031-29-1
(-)-dimethy-2,3-O-isopropylidene-L-tartrate

: 124-40-3
dimethyl amine

: 63126-29-4,74752-95-7
(4R,5R)-2,2,N,N,N',N'-hexamethyl-1,3-dioxolane-4,5-dicarboxamide

Guidance literature:: In methanol; for 96h; Ambient temperature;
DOI:10.1002/hlca.19940770802

Reference yield: 90.0%

: 26549-65-5
N,N,N',N'-tetramethyl L-tartramide

: 77-76-9
2,2-dimethoxy-propane

: 63126-29-4,74752-95-7
(4R,5R)-2,2,N,N,N',N'-hexamethyl-1,3-dioxolane-4,5-dicarboxamide

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 0.5h; Heating;
DOI:10.1021/jo00250a037

Reference yield:

: 77-76-9
2,2-dimethoxy-propane

: 63126-29-4,74752-95-7
(4R,5R)-2,2,N,N,N',N'-hexamethyl-1,3-dioxolane-4,5-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid

2: methanol

With toluene-4-sulfonic acid; In methanol;
DOI:10.1007/s00706-011-0588-1