N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide

Base Information

Chemical Name:N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide
CAS No.:1422695-63-3
Molecular Formula:C₁₇H₁₉N₅O₄S
Molecular Weight:389.435
Hs Code.:

Synonyms:N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide

Chemical Property:

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Technology Process of N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide

There total 4 articles about N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 350688-28-7
C₁₆H₁₆N₄O₄S

: 141-43-5
ethanolamine

: 1422695-63-3
N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide

Guidance literature:: With pyridine; at 90 - 100 ℃; for 3h;
DOI:10.1016/j.ejmech.2012.11.005

Reference yield:

: 162976-69-4,102040-01-7,110342-67-1,212384-28-6,276680-08-1,63090-40-4,63278-70-6,59758-95-1
1H-benzimidazol-2-ylcarbamic acid methyl ester

: 1422695-63-3
N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: chlorosulfonic acid / ethyl acetate / 0 °C

2: triethylamine / tetrahydrofuran / 20 °C

3: pyridine / 3 h / 90 - 100 °C

With pyridine; chlorosulfonic acid; triethylamine; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.ejmech.2012.11.005

Reference yield:

: 79213-74-4
methyl [6-(chlorosulfonyl)-1H-benzo[d]imidazol-2-yl]-carbamate

: 1422695-63-3
N-benzyl-2-(3-(2-hydroxyethyl)ureido)-1H-benzo[d]imidazole-5-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 20 °C

2: pyridine / 3 h / 90 - 100 °C

With pyridine; triethylamine; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2012.11.005