methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

Base Information

Chemical Name:methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside
CAS No.:402759-14-2
Molecular Formula:C₇₀H₇₈O₁₇
Molecular Weight:1191.38
Hs Code.:

Synonyms:methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

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Chemical Property of methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

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Technology Process of methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

There total 1 articles about methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-2-O-benzoyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

: 402759-14-2
methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 8h;
DOI:10.1021/ja029302m

Reference yield: 88.0%

: 1448225-46-4
ethyl 2,3-di-O-benzyl-5-O-(2-quinolinecarbonyl)-1-thio-α-D-arabinofuranoside

: 402759-14-2
methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

: 1448225-81-7
methyl 5-O-{3,5-di-O-(2-O-[2,3-di-O-benzyl-5-O-(2-quinolinecarbonyl)-β-D-arabinofuranosyl]-3,5-di-O-benzyl-α-D-arabinofuransoyl)-2-O-benzyl-α-D-arabinofuranosyl}-2,3-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In 1,2-dichloro-ethane; at -30 - 30 ℃; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol401755e

Reference yield: 74.0%

: 527680-88-2
Benzoic acid (1S,2R,4R,5S)-4-(toluene-4-sulfinyl)-3,6-dioxa-bicyclo[3.1.0]hex-2-ylmethyl ester

: 402759-14-2
methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside

: 527682-43-5
methyl 5-O-{3,5-di-O-(2-O-[2,3-anhydro-5-O-benzoyl-β-D-arabinofuranosyl]-3,5-di-O-benzyl-α-D-arabinofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl}-2,3-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: Benzoic acid (1S,2R,4R,5S)-4-(toluene-4-sulfinyl)-3,6-dioxa-bicyclo[3.1.0]hex-2-ylmethyl ester; With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; In dichloromethane; at -40 ℃; for 0.166667h;

methyl 5-O-[3,5-di-O-(3,5-di-O-benzyl-α-D-arabionofuranosyl)-2-O-benzyl-α-D-arabinofuranosyl]-2,3-di-O-benzyl-α-D-arabinofuranoside; In dichloromethane;
DOI:10.1021/ja029302m