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Technology Process of (C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6]

(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6]

Base Information
  • Chemical Name:(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6]
  • CAS No.:250655-46-0
  • Molecular Formula:C26H25Cl2N4OOs*F6P
  • Molecular Weight:815.581
  • Hs Code.:
(C<sub>5</sub>H<sub>4</sub>NC<sub>5</sub>H<sub>3</sub>NC<sub>5</sub>H<sub>4</sub>N)OsCl<sub>2</sub>(CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CHNC(CH<sub>3</sub>)2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[(C<sub>5</sub>H<sub>4</sub>NC<sub>5</sub>H<sub>3</sub>NC<sub>5</sub>H<sub>4</sub>N)OsCl<sub>2</sub>(CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CHNC(CH<sub>3</sub>)2)][PF<sub>6</sub>]

Synonyms:(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6]

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Chemical Property of (C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6]
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Technology Process of (C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6]

There total 2 articles about (C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

cis-[(terpy)OsCl2(1,2-η(2)-PhCHNCHPh)]PF6
250655-35-7

cis-[(terpy)OsCl2(1,2-η(2)-PhCHNCHPh)]PF6

1-methoxy-4-(2-methylallyl)benzene
20849-82-5

1-methoxy-4-(2-methylallyl)benzene

(C<sub>5</sub>H<sub>4</sub>NC<sub>5</sub>H<sub>3</sub>NC<sub>5</sub>H<sub>4</sub>N)OsCl<sub>2</sub>(CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CHNC(CH<sub>3</sub>)2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[(C<sub>5</sub>H<sub>4</sub>NC<sub>5</sub>H<sub>3</sub>NC<sub>5</sub>H<sub>4</sub>N)OsCl<sub>2</sub>(CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CHNC(CH<sub>3</sub>)2)][PF<sub>6</sub>]
250655-46-0

(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)(1+)*PF6(1-)=[(C5H4NC5H3NC5H4N)OsCl2(CH3OC6H4CHNC(CH3)2)][PF6]

Guidance literature:
In acetonitrile;
DOI:10.1021/ja992385v

Reference yield: 71.0%

cis-[Os(VI)(2,2':6',2''-terpyridine)(Cl)2(N)](PF<sub>6</sub>)
127571-48-6,159248-17-6

cis-[Os(VI)(2,2':6',2''-terpyridine)(Cl)2(N)](PF6)

1-methoxy-4-(2-methyl-1-propenyl)benzene
877-99-6

1-methoxy-4-(2-methyl-1-propenyl)benzene

cis-[(2,2':6',2''-terpyridine)OsCl2(1,2-η2-[4-MeOC6H4]CH=N=CMe2)]PF6
250655-46-0

cis-[(2,2':6',2''-terpyridine)OsCl2(1,2-η2-[4-MeOC6H4]CH=N=CMe2)]PF6

Guidance literature:
In acetonitrile; soln. of Os-complex and ligand in MeCN was added into flask, allowed to stand at room temp. for 48 h under N2 or Ar; MeCN was evapd. on rotary evaporator, washed with ether, allowed to stand overnight, filtered, washed with Et2O, dried in air; elem. anal.;
DOI:10.1021/om034404m
upstream raw materials:

cis-[(terpy)OsCl2(1,2-η(2)-PhCHNCHPh)]PF6

1-methoxy-4-(2-methylallyl)benzene

cis-[Os(VI)(2,2':6',2''-terpyridine)(Cl)2(N)](PF6)

1-methoxy-4-(2-methyl-1-propenyl)benzene

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