4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

Base Information

Chemical Name:4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid
CAS No.:1379147-88-2
Molecular Formula:C₁₅H₆Cl₃NO₄
Molecular Weight:370.576
Hs Code.:

Synonyms:4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

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Chemical Property of 4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

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Technology Process of 4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

There total 1 articles about 4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 942-06-3
4,5-dichlorophthalic anhydride

: 89-77-0
2-Amino-4-chlorobenzoic acid

: 1379147-88-2
4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

Guidance literature:: With acetic acid; at 110 ℃; for 16h;
DOI:10.1039/c2ob25314c

Reference yield:

: 1379147-88-2
4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

: 1379147-91-7
4-chloro-2-(5,6-dichloro-1,3-dioxoisoindolin-2-yl)benzoyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1039/c2ob25314c

Reference yield:

: 1379147-88-2
4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

: 1379148-08-9
diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

: 1379148-09-0
diethyl 3,8,9-trichloro-6-oxo-6H-isoindolo[2,1-a]indol-11-ylphosphate

: 1379148-10-3
C₁₉H₁₅Cl₃NO₆P

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 16 h / 20 °C

2: dichloromethane / 24 h / Reflux

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c2ob25314c