diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

Base Information

Chemical Name:diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate
CAS No.:1379148-08-9
Molecular Formula:C₁₉H₁₅Cl₃NO₅P
Molecular Weight:474.665
Hs Code.:

Synonyms:diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

Chemical Property:

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Technology Process of diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

There total 4 articles about diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1379147-91-7
4-chloro-2-(5,6-dichloro-1,3-dioxoisoindolin-2-yl)benzoyl chloride

: 122-52-1
triethyl phosphite

: 78-40-0
triethyl phosphate

: 1379148-08-9
diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

: 1379148-09-0
diethyl 3,8,9-trichloro-6-oxo-6H-isoindolo[2,1-a]indol-11-ylphosphate

: 1379148-11-4
C₂₃H₂₆Cl₃NO₉P₂

Guidance literature:: In toluene; at 100 ℃; for 3.03333h;
DOI:10.1039/c2ob25314c

Reference yield:

: 1379147-88-2
4-chloro-2-(5,6-dichloro-1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)benzoic acid

: 1379148-08-9
diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

: 1379148-09-0
diethyl 3,8,9-trichloro-6-oxo-6H-isoindolo[2,1-a]indol-11-ylphosphate

: 1379148-10-3
C₁₉H₁₅Cl₃NO₆P

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 16 h / 20 °C

2: dichloromethane / 24 h / Reflux

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c2ob25314c

Reference yield:

: 942-06-3
4,5-dichlorophthalic anhydride

: 1379148-08-9
diethyl (3,8,9-trichloro-6,11-dioxo-6H-isoindolo[2,1-a]indol-10b(11H)-yl)phosphonate

: 1379148-09-0
diethyl 3,8,9-trichloro-6-oxo-6H-isoindolo[2,1-a]indol-11-ylphosphate

: 1379148-10-3
C₁₉H₁₅Cl₃NO₆P

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 16 h / 110 °C

2: thionyl chloride; N,N-dimethyl-formamide / 16 h / 20 °C

3: dichloromethane / 24 h / Reflux

With thionyl chloride; acetic acid; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c2ob25314c