Technology Process of 2,3-epoxy-2-(2-nitrophenyl)propionaldehyde
There total 2 articles about 2,3-epoxy-2-(2-nitrophenyl)propionaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; dihydrogen peroxide;
In
methanol;
at 10 ℃;
for 1h;
addition at -5 to 0 deg C;
DOI:10.1246/bcsj.62.4061
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / trifluoroacetic acid, dicyclohexylcarbodiimide, pyridine / benzene; dimethylsulfoxide / 2 h / Ambient temperature
2: 93 percent / aq. 31percent H2O2, aq. 24percent NaOH / methanol / 1 h / 10 °C / addition at -5 to 0 deg C
With
pyridine; sodium hydroxide; dihydrogen peroxide; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
methanol; dimethyl sulfoxide; benzene;
DOI:10.1246/bcsj.62.4061
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
acetic anhydride;
under 760 Torr;
Ambient temperature;
DOI:10.1246/bcsj.62.4061
