Benzyl-phenyl-sulfamic acid ethyl ester

Base Information

Chemical Name:Benzyl-phenyl-sulfamic acid ethyl ester
CAS No.:104254-92-4
Molecular Formula:C₁₅H₁₇NO₃S
Molecular Weight:291.371
Hs Code.:

Synonyms:Benzyl-phenyl-sulfamic acid ethyl ester

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Chemical Property of Benzyl-phenyl-sulfamic acid ethyl ester

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Technology Process of Benzyl-phenyl-sulfamic acid ethyl ester

There total 2 articles about Benzyl-phenyl-sulfamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 3782-61-4
ethyl phenylamidosulfate

: 100-44-7
benzyl chloride

: 104254-92-4
Benzyl-phenyl-sulfamic acid ethyl ester

Guidance literature:: With sodium carbonate; N-benzyl-N,N,N-triethylammonium chloride; at 20 ℃; for 0.666667h;
DOI:10.1055/s-1985-31390

Reference yield:

: 60260-49-3
phenylsulfamyl chloride

: 104254-92-4
Benzyl-phenyl-sulfamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Na₂CO₃ / tetra-n-butylammonium bromide / benzene / 1 h / Ambient temperature

2: 44 percent / Na₂CO₃ / benzyltriethylammonium chloride / 0.67 h / 20 °C

With sodium carbonate; tetrabutylammomium bromide; N-benzyl-N,N,N-triethylammonium chloride; In benzene;
DOI:10.1055/s-1985-31390