<4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

Base Information

Chemical Name:<4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane
CAS No.:135782-07-9
Molecular Formula:C₂₂H₆Cl₁₃NO₂
Molecular Weight:777.184
Hs Code.:

Synonyms:<4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

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Technology Process of <4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

There total 13 articles about <4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 135782-06-8
(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

: 107-18-6
allyl alcohol

: 135782-07-9
<4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

Guidance literature:: With dmap; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1039/P19910001101

Reference yield:

: 10469-02-0
3,4,5,6-tetrachloro-2-methylpyridine

: 135782-07-9
<4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

Guidance literature:: Multi-step reaction with 12 steps

1: 60.5 percent Chromat_. / Cl₂ / CCl₄ / 0.5 h / Heating; Irradiation

2: 78 percent / AlCl₃ / 18 h / Heating

3: 84 percent / Cl₂ / CCl₄ / 1 h / Heating; Irradiation

4: 84 percent / conc. H₂SO₄ / 0.5 h / Ambient temperature

5: 44 percent / diethyl ether / 2 h / Heating

6: 90 percent / 57percent aq. HI / hexane / 4 h / Heating

7: 60 percent / S₂Cl₂, AlCl₃, SO₂Cl₂ / 2 h / Heating

8: 91 percent / Cl₂ / CCl₄ / 35 h / Heating; Irradiation

9: 96 percent / 30percent oleum, water / 24 h / Ambient temperature

10: 86 percent / KMnO₄ / acetone / 2 h / Heating

11: 97 percent / SOCl₂ / 24 h / Heating

12: 89 percent / dimethylaminopyridine / CH₂Cl₂ / 24 h / Ambient temperature

With disulfur dichloride; dmap; potassium permanganate; aluminium trichloride; thionyl chloride; sulfuryl dichloride; sulfuric acid; water; hydrogen iodide; chlorine; In tetrachloromethane; diethyl ether; hexane; dichloromethane; acetone;
DOI:10.1039/P19910001101

Reference yield:

: 38373-64-7
2-benzoyltetrachloropyridine

: 135782-07-9
<4-(allyloxycarbnyl)tetrachlorophenyl>(pentachlorophenyl)(tetrachloro-2-pyridyl)methane

Guidance literature:: Multi-step reaction with 8 steps

1: 44 percent / diethyl ether / 2 h / Heating

2: 90 percent / 57percent aq. HI / hexane / 4 h / Heating

3: 60 percent / S₂Cl₂, AlCl₃, SO₂Cl₂ / 2 h / Heating

4: 91 percent / Cl₂ / CCl₄ / 35 h / Heating; Irradiation

5: 96 percent / 30percent oleum, water / 24 h / Ambient temperature

6: 86 percent / KMnO₄ / acetone / 2 h / Heating

7: 97 percent / SOCl₂ / 24 h / Heating

8: 89 percent / dimethylaminopyridine / CH₂Cl₂ / 24 h / Ambient temperature

With disulfur dichloride; dmap; potassium permanganate; aluminium trichloride; thionyl chloride; sulfuryl dichloride; sulfuric acid; water; hydrogen iodide; chlorine; In tetrachloromethane; diethyl ether; hexane; dichloromethane; acetone;
DOI:10.1039/P19910001101