C₃₄H₄₅NO₃Si

Base Information

Chemical Name:C₃₄H₄₅NO₃Si
CAS No.:950206-50-5
Molecular Formula:C₃₄H₄₅NO₃Si
Molecular Weight:543.822
Hs Code.:

C<sub>34</sub>H<sub>45</sub>NO<sub>3</sub>Si

Synonyms:C₃₄H₄₅NO₃Si

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Chemical Property of C₃₄H₄₅NO₃Si

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Technology Process of C₃₄H₄₅NO₃Si

There total 8 articles about C₃₄H₄₅NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 950206-49-2
C₂₉H₃₇NOSi

: 24424-99-5
di-tert-butyl dicarbonate

: 950206-50-5
C₃₄H₄₅NO₃Si

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1055/s-2007-982577

Reference yield:

: 950206-45-8
C₂₉H₃₆O₄SSi

: 950206-50-5
C₃₄H₄₅NO₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 73 percent / NaN₃ / dimethylformamide / 80 °C

2.1: PPh₃; methanol / 20 °C

2.2: 62 percent / Et₃N; DMAP / CH₂Cl₂; methanol / 0 - 20 °C

3.1: 75 percent / Grubbs' first-generation catalyst / CH₂Cl₂ / Heating

4.1: 86 percent / H₂ / Pd/C / 20 °C

5.1: BH₃*DMS / tetrahydrofuran / 0 - 20 °C

5.2: 82 percent / ethanol / Heating

6.1: 85 percent / Et₃N / tetrahydrofuran / 0 - 20 °C

With methanol; sodium azide; dimethylsulfide borane complex; hydrogen; triethylamine; triphenylphosphine; palladium on activated charcoal; Grubbs catalyst first generation; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2.1: Staudinger reaction;
DOI:10.1055/s-2007-982577

Reference yield:

: 950206-47-0
C₂₉H₃₃NO₂Si

: 950206-50-5
C₃₄H₄₅NO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / H₂ / Pd/C / 20 °C

2.1: BH₃*DMS / tetrahydrofuran / 0 - 20 °C

2.2: 82 percent / ethanol / Heating

3.1: 85 percent / Et₃N / tetrahydrofuran / 0 - 20 °C

With dimethylsulfide borane complex; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1055/s-2007-982577