methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

Base Information

Chemical Name:methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate
CAS No.:87043-00-3
Molecular Formula:C₂₀H₂₂N₂O₄S
Molecular Weight:386.472
Hs Code.:

Synonyms:methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

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Chemical Property of methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

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Technology Process of methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

There total 3 articles about methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 59830-60-3
benzyl (1S)-(1-formyl-2-phenylethyl)carbamate

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 87043-00-3
methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

Guidance literature:: With sulfur; sodiumsulfide nonahydrate; copper dichloride; In tetrahydrofuran; at 50 ℃; for 10h; Schlenk technique;
DOI:10.1021/acs.orglett.1c03370

Reference yield: 84.0%

: 5184-17-8,21685-41-6,4818-07-9
N-benzyloxycarbonyl-L-phenylalanylglycine methyl ester

: 87043-00-3
methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

Guidance literature:: With Lawessons reagent; In toluene; at 95 - 100 ℃; for 2h; Method for preparation of N-protected endothiopeptides;
DOI:10.1016/S0040-4020(01)91869-1

Reference yield:

: 59830-60-3
benzyl (1S)-(1-formyl-2-phenylethyl)carbamate

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 87043-00-3
methyl (S)-(2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

: methyl (2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioyl)glycinate

Guidance literature:: With sulfur; sodiumsulfide nonahydrate; copper dichloride; In tetrahydrofuran; at 50 ℃; for 12h; Reagent/catalyst; Solvent; Overall yield = 80 percent; Overall yield = 308.8 mg; Catalytic behavior; Schlenk technique;
DOI:10.1021/acs.orglett.1c03370