4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole

Base Information

Chemical Name:4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole
CAS No.:1268314-62-0
Molecular Formula:C₁₇H₁₈BrN₃O
Molecular Weight:360.253
Hs Code.:

Synonyms:4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole

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Chemical Property of 4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole

Chemical Property:

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Technology Process of 4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole

There total 11 articles about 4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 908288-77-7
4-bromo-1-(2,2-dimethylpropyl)-1H-1,2,3-benzotriazol-5-ol

: 98-80-6
phenylboronic acid

: 1268314-62-0
4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole

Guidance literature:: With copper diacetate; triethylamine; In dichloromethane; at 20 ℃; for 18h; Molecular sieve;

Reference yield:

: 5813-64-9
2.2-dimethylpropylamine

: 1268314-62-0
4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethyl sulfoxide / 48 h / 120 °C

1.2: 0.33 h / 20 °C

1.3: pH 7

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 20 °C / 760.05 Torr / Inert atmosphere

3.1: water; sodium nitrite; sulfuric acid / 20 - 120 °C / microwave irradiation

4.1: pyridinium hydrobromide perbromide / chloroform / 20 °C

5.1: triethylamine; copper diacetate / dichloromethane / 18 h / 20 °C / Molecular sieve

With pyridinium hydrobromide perbromide; sulfuric acid; water; hydrogen; copper diacetate; triethylamine; sodium nitrite; palladium 10% on activated carbon; In ethanol; dichloromethane; chloroform; dimethyl sulfoxide;

Reference yield:

: 630-19-3
pivalaldehyde

: 1268314-62-0
4-bromo-1-(2,2-dimethylpropyl)-5-phenoxy-1H-benzotriazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C / Inert atmosphere

3.1: sodium nitrite; acetic acid / water / 0 - 20 °C

3.2: 20 °C

3.3: pH 10

4.1: boron tribromide / dichloromethane / 0 - 20 °C

4.2: pH 7

5.1: triethylamine; copper diacetate / dichloromethane / 18 h / 20 °C / Molecular sieve

With hydrogen; copper diacetate; boron tribromide; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; sodium nitrite; palladium 10% on activated carbon; In ethanol; dichloromethane; water;