{(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate

Base Information

Chemical Name:{(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate
CAS No.:1207529-80-3
Molecular Formula:C₁₃H₂₂F₃NO₅S
Molecular Weight:361.383
Hs Code.:

Synonyms:{(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate

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Chemical Property of {(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of {(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate

There total 4 articles about {(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 239074-29-4
trans (4-hydroxymethyl-cyclohexyl)-carbamic acid tert-butyl ester

: 358-23-6
trifluoromethylsulfonic anhydride

: 1207529-80-3
{(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1207529-80-3
{(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / methanol / 10 - 20 °C

2.1: sodium tetrahydroborate; ethanol; calcium chloride / tetrahydrofuran / 5 - 20 °C

2.2: 10 °C / pH 11

3.1: pyridine / dichloromethane / 1 h / 0 °C

With pyridine; sodium tetrahydroborate; ethanol; triethylamine; calcium chloride; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 146307-51-9
methyl (1R,4R)-4-((tert-butoxycarbonyl)amino)cyclohexane-1-carboxylate

: 1207529-80-3
{(1r,4r)-4-[(tert-butoxycarbonyl)amino]cyclohexyl}methyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate; ethanol; calcium chloride / tetrahydrofuran / 5 - 20 °C

1.2: 10 °C / pH 11

2.1: pyridine / dichloromethane / 1 h / 0 °C

With pyridine; sodium tetrahydroborate; ethanol; calcium chloride; In tetrahydrofuran; dichloromethane;