methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate

Base Information

• Chemical Name: methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate
• CAS No.: 118799-86-3
• Molecular Formula: C₂₁H₂₂O₇
• Molecular Weight: 386.401

Synonyms:methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate

Chemical Property of methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate

Chemical Property:

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Technology Process of methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate

There total 12 articles about methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(E)-methyl 3-<(2RS,3SR)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-7-methoxy-3-methoxycarbonyl-1-benzofuran-5-yl>-1-propenoate (118799-80-7) → methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate (118799-86-3)

Guidance literature:

With lithium borohydride; In tetrahydrofuran; at -78 - 20 ℃; for 2.5h;

DOI:10.1016/j.bmc.2007.06.047

Reference yield: 73.0%

Methyl (E)-3-[2-(4-acetoxy-3-methoxyphenyl)-3-acetoxymethyl-7-methoxy-2,3-dihydrobenzo[b]furan-5-yl]propenoate → methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate (118799-86-3)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; Saponification;

DOI:10.1016/S0040-4039(00)00187-8

Reference yield: 71.0%

Methyl (E)-3-[2-(3-methoxy-4-methoxymethoxyphenyl)-3-methoxymethoxymethyl-7-methoxy-2,3-dihydrobenzo[b]furan-5-yl]propenoate → methyl (E)-3-<(2R*,3S*)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-3-hydroxymethyl-7-methoxy-1-benzofuran-5-yl>propenoate (118799-86-3)

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃;

DOI:10.1016/S0040-4039(00)00187-8

upstream raw materials:

methyl (E)-3-<(2R*,3S*)-2,3-dihydro-3-hydroxymethyl-7-methoxy-2-(3-methoxy-4-methoxymethoxyphenyl)-1-benzofuran-5-yl>propenoate

(E)-methyl 3-<(2RS,3SR)-2,3-dihydro-2-(4-hydroxy-3-methoxyphenyl)-7-methoxy-3-methoxycarbonyl-1-benzofuran-5-yl>-1-propenoate

2-(2-benzyloxy-5-bromo-3-methoxy-phenyl)-1-(4-benzyloxy-3-methoxy-phenyl)-propane-1,3-diol

Methyl ferulate

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