{Re2(μ-H)4H4(triphenylphosphine)4}PF6

Base Information

• Chemical Name: {Re2(μ-H)4H4(triphenylphosphine)4}PF6
• CAS No.: 86664-86-0
• Molecular Formula: C₇₂H₆₈P₄Re₂*F₆P
• Molecular Weight: 1574.61
• Mol file: 86664-86-0.mol

Synonyms:{Re2(μ-H)4H4(triphenylphosphine)4}PF6

Chemical Property of {Re2(μ-H)4H4(triphenylphosphine)4}PF6

Chemical Property:

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Technology Process of {Re2(μ-H)4H4(triphenylphosphine)4}PF6

There total 1 articles about {Re2(μ-H)4H4(triphenylphosphine)4}PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

Re2(μ-H)4H4(triphenylphosphine)4 + tropylium hexafluorophosphate (29663-54-5) → {Re2(μ-H)4H4(triphenylphosphine)4}PF6 (86664-86-0)

Guidance literature:

In dichloromethane; under N2, dropwise addn. of C7H7PF6 in CH2Cl2 to Re-compd. in CH2Cl2 at 0°C with stirring, stirred for 5 min; removal of solvent under vac., stirred under diethyl ether, filtered off, washed with diethyl ether, dried in vac.; elem. anal.;

DOI:10.1021/ja00313a033

upstream raw materials:

tropylium hexafluorophosphate