(2R,3S,4R,5S,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol

Base Information

• Chemical Name: (2R,3S,4R,5S,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol
• CAS No.: 131227-80-0
• Molecular Formula: C₂₈H₃₃NO₅
• Molecular Weight: 463.574

Synonyms:(2R,3S,4R,5S,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol

Chemical Property of (2R,3S,4R,5S,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol

Chemical Property:

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Technology Process of (2R,3S,4R,5S,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol

There total 3 articles about (2R,3S,4R,5S,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

bromo-triphenyl-methane (596-43-0) + Methyl 2-deoxy-2-(N,N-dimethylamino)-α-D-glucopyranoside (131227-79-7) → (2R,3S,4R,5R,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol (131227-80-0)

Guidance literature:

In pyridine; at 80 ℃; for 12h;

DOI:10.1016/S0040-4020(01)87751-6

Reference yield:

bromo-triphenyl-methane (596-43-0) + Methyl 2-deoxy-2-(N,N-dimethylamino)-α-D-mannopyranoside (131227-84-4) → (2R,3S,4R,5S,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol (131227-80-0)

Guidance literature:

With pyridine; at 80 ℃;

DOI:10.1016/S0040-4020(01)87751-6

Reference yield:

bromo-triphenyl-methane (596-43-0) + Methyl-2-deoxy-2-(N,N-dimethylamino)-α-D-galactopyranoside (131227-83-3) → (2R,3R,4R,5R,6S)-5-Dimethylamino-6-methoxy-2-trityloxymethyl-tetrahydro-pyran-3,4-diol (131227-80-0)

Guidance literature:

With pyridine; at 80 ℃;

DOI:10.1016/S0040-4020(01)87751-6

upstream raw materials:

bromo-triphenyl-methane

Methyl-2-deoxy-2-(N,N-dimethylamino)-α-D-galactopyranoside

Methyl 2-deoxy-2-(N,N-dimethylamino)-α-D-mannopyranoside

Methyl 2-deoxy-2-(N,N-dimethylamino)-α-D-glucopyranoside

Downstream raw materials:

Methyl-2-deoxy-2-(N-formyl N-methyl)-α-D-glucopyranoside 6-acetate 3,4-diphenylbenzoate

Methyl 2-deoxy-2-(N,N-dimethylamino)-3,4-O-diphenylbenzyl-α-D-gluco-pyranoside

Methyl-2-deoxy-2-(N-formyl N-methyl)-α-D-mannopyranoside 6-acetate 3,4-diphenylbenzoate

Methyl-2-deoxy-2-(N-formyl N-methyl)-3-O-methyl-α-D-mannopyranoside 4,6-diphenylbenzoate

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