Methanimidamide,N,N'-bis(2-chlorophenyl)-

Base Information

• Chemical Name: Methanimidamide,N,N'-bis(2-chlorophenyl)-
• CAS No.: 30881-04-0
• Molecular Formula: C13H10 Cl2 N2
• Molecular Weight: 265.142
• Mol file: 30881-04-0.mol

Synonyms:Formamidine,N,N'-bis(o-chlorophenyl)- (6CI,7CI,8CI); N,N'-Bis(2-chlorophenyl)formamidine;NSC 229471

Chemical Property of Methanimidamide,N,N'-bis(2-chlorophenyl)-

Chemical Property:

• Boiling Point: 384.2°Cat760mmHg
• Flash Point: 186.2°C
• Density: 1.24g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanimidamide,N,N'-bis(2-chlorophenyl)-

There total 7 articles about Methanimidamide,N,N'-bis(2-chlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

orthoformic acid triethyl ester (122-51-0) + o-chloroaniline (95-51-2) → N,N’-bis(2-chlorophenyl)formamidine (30881-04-0)

Guidance literature:

With mesoporous nanocomposite of Fe₃O₄ and -NHSO₃H functionalized silica (MCM-41); In neat (no solvent); at 90 ℃; for 0.5h;

DOI:10.1080/00304948.2020.1870398

Reference yield: 74.0%

o-chloroaniline (95-51-2) + trimethyl orthoformate (149-73-5) → N,N’-bis(2-chlorophenyl)formamidine (30881-04-0)

Guidance literature:

With choline chloride*2SnCl₂; at 90 ℃;

DOI:10.1016/j.crci.2012.06.011

Reference yield: 54.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + o-chloroaniline (95-51-2) → N,N’-bis(2-chlorophenyl)formamidine (30881-04-0)

Guidance literature:

With sodium hydroxide; trimethylsilyl bromide; In dichloromethane; at 0 ℃;

upstream raw materials:

orthoformic acid triethyl ester

o-chloroaniline

N-(2-chloro-phenyl)-formimidic acid ethyl ester

N,N-dimethyl-formamide

Downstream raw materials:

2-(2-Chlor-anilinomethylen)-2,3-dihydro-3-oxo-benzo-thiophen-1,1-dioxid

2-(2-Chlor-anilinomethylen)-2,3-dihydro-3-oxo-benzo-thiophen-1,1-dioxid

trans-bis(N,N'-di-o-chlorophenylformamidinate)bis(acetate)dichromium(II)

4-[1-(2-Chloro-phenylamino)-meth-(Z)-ylidene]-2,5-dimethyl-2,4-dihydro-pyrazol-3-one

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