(3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione

Base Information

• Chemical Name: (3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione
• CAS No.: 1192030-87-7
• Molecular Formula: C₄₀H₃₉NO₇Si
• Molecular Weight: 673.838

Synonyms:(3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione

Chemical Property of (3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione

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Technology Process of (3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione

There total 1 articles about (3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C40H41NO7Si (1192030-85-5) → (3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione (1192030-87-7)

Guidance literature:

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In acetonitrile; at 50 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ja9073694

Reference yield: 9.0%

2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one (1192030-58-2) + (3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione (1192030-87-7) → C65H64FNO12Si (1192030-89-9)

Guidance literature:

2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione; With di-n-butylboryl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; at -78 - 25 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja9073694

upstream raw materials:

C₄₀H₄₁NO₇Si

Downstream raw materials:

C₆₅H₆₄FNO₁₂Si

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