2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

Base Information

Chemical Name:2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one
CAS No.:1192030-58-2
Molecular Formula:C₂₅H₂₅FO₅
Molecular Weight:424.469
Hs Code.:

Synonyms:2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

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Chemical Property of 2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

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Technology Process of 2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

There total 1 articles about 2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1192030-57-1
9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

: 1192030-58-2
2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

Guidance literature:: 9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

With N-fluorobis(benzenesulfon)imide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja9073694

Reference yield: 11.0%

: 1192030-58-2
2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

: 1192030-86-6
(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

: 1192030-88-8
C₆₅H₆₅FO₁₀Si

Guidance literature:: 2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione; With di-n-butylboryl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; at -78 - 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja9073694

Reference yield: 9.0%

: 1192030-58-2
2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

: 1192030-87-7
(3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione

: 1192030-89-9
C₆₅H₆₄FNO₁₂Si

Guidance literature:: 2-fluoro-9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(3R,4R)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-8-(4-nitrobenzyloxy)-3,4-dihydroanthracene-1,9,10(2H)-trione; With di-n-butylboryl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; at -78 - 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja9073694