5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine

Base Information

Chemical Name:5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine
CAS No.:160905-88-4
Molecular Formula:C₃₉H₄₈N₆O₉Si
Molecular Weight:772.93
Hs Code.:

Synonyms:5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine

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Technology Process of 5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine

There total 4 articles about 5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.6%

: 123-76-2
levulinic acid

: 160905-87-3
5'-O-[(tert-butyl)diphenylsilyl]-2-[(dimethylamino)methylidene]guanosine

: 160905-88-4
5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 118-00-3
G

: 160905-88-4
5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / Ambient temperature

2: methanol

3: 92.6 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / tetrahydrofuran; CH₂Cl₂

With 1H-imidazole; dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 160905-88-4
5'-O-(tert-butyldiphenylsilyl)-2-N-dimethylaminomethylene-2',3'-di-O-laevulinylguanosine

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / Ambient temperature

2: methanol

3: 92.6 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / tetrahydrofuran; CH₂Cl₂

With 1H-imidazole; dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;