(3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane

Base Information

Chemical Name:(3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane
CAS No.:1378432-39-3
Molecular Formula:C₁₅H₂₃Br₂FOSi
Molecular Weight:426.239
Hs Code.:

Synonyms:(3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane

Chemical Property:

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Technology Process of (3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane

There total 1 articles about (3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1378432-36-0
3-(2-bromo-3-fluorophenyl)-3-(tert-butyldimethylsilyloxy)propan-1-ol

: 1378432-39-3
(3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

Reference yield: 91.0%

: 691856-35-6
5-cyclopropyl-2-(4-fluorophenyl)-N-methyl-6-(methylsulfonamido)benzofuran-3-carboxamide

: 1378432-39-3
(3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane

: 1378432-42-8
6-(N-(3-(2-bromo-3-fluorophenyl)-3-(tert-butyldimethylsilyloxy)propyl)methylsulfonamido)-5-cyclopropyl-2-(4-fluorophenyl)-N-methylbenzofuran-3-carboxamide

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 2h; Inert atmosphere;

Reference yield:

: 1378432-39-3
(3-bromo-1-(2-bromo-3-fluorophenyl)propoxy)(tert-butyl)dimethylsilane

: 1378428-21-7
5-cyclopropyl-6-(N-(2-(7-fluoro-1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)ethyl)methylsulfonamido)-2-(4-fluorophenyl)-N-methylbenzofuran-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

2: hydrogenchloride / water; tetrahydrofuran / 40 °C / Inert atmosphere

3: potassium fluoride / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 1.5 h / 120 °C / Inert atmosphere

With hydrogenchloride; potassium fluoride; potassium carbonate; potassium iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;