(Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate

Base Information

Chemical Name:(Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate
CAS No.:1202946-82-4
Molecular Formula:C₂₀H₁₉N₇O₃
Molecular Weight:405.416
Hs Code.:

Synonyms:(Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate

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Chemical Property of (Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate

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Technology Process of (Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate

There total 7 articles about (Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₁₉F₃N₄O₆S

: 1202946-82-4
(Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate

Guidance literature:: With sodium azide; In acetonitrile; at 50 ℃; for 2h;

Reference yield:

: 74-87-3
methylene chloride

: 1346110-70-0
but-3-yn-1-yl {6-[({[(Z)-phenyl(1H-tetrazol-5-yl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

: 1202946-82-4
(Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate

: but-3-yn-1-yl {6-[({[(Z)-(2-methyl-2H-tetrazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}carbamate

Guidance literature:: With caesium carbonate; In tert-butyl methyl ether; acetonitrile; at 60 ℃; for 5h;

Reference yield:

: 83490-71-5
N?methyl?2?oxo?2?phenylacetamide

: 1202946-82-4
(Z)-but-3-yn-1-yl (6-(((((1-methyl-1H-tetrazol-5-yl)(phenyl)methylene)amino)oxy)methyl)pyridin-2-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; pyridine / 10 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 3.5 h / 20 °C

3.1: pyridine / acetonitrile / 50 °C / Cooling with ice

4.1: sodium azide / acetonitrile / 2 h / 50 °C

With pyridine; sodium azide; hydroxylamine hydrochloride; sodium hydride; In N,N-dimethyl-formamide; acetonitrile;