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Product FOB Price Min.Order Supply Ability Supplier
Chloromethane
Cas No: 74-87-3
USD $ 1.0-2.0 / Metric Ton 1 Metric Ton 100 Metric Ton/Week Hebei yanxi chemical co.,LTD. Contact Supplier
Amadis Chemical offer CAS#74-87-3;CAT#A865788
Cas No: 74-87-3
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
Chloromethane
Cas No: 74-87-3
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
Methyl chloride Manufacturer/High quality/Best price/In stock
Cas No: 74-87-3
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
METHYL CHLORIDE
Cas No: 74-87-3
USD $ 20.0-20.0 / Kilogram 1 Kilogram 1 Metric Ton/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
Superior Purity Chloromethane CAS NO.74-87-3
Cas No: 74-87-3
USD $ 1.0-2.0 / Gram 10 Gram 100 Metric Ton/Day Jilin Tely Imp.& Exp.Co., Ltd. Contact Supplier
Methane, chloro-
Cas No: 74-87-3
USD $ 100.0-150.0 / Kilogram 1 Kilogram 1000 Metric Ton/Day Wuhan Monad Medicine Tech Co.,LTD Contact Supplier
74-87-3 CH3Cl METHYL CHLORIDE CAS NO.74-87-3
Cas No: 74-87-3
No Data 10 Gram 500 Kilogram/Month Changchun Artel lmport and Export trade company Contact Supplier
METHYL CHLORIDE
Cas No: 74-87-3
USD $ 1.0-1.0 / Gram 1 Gram 120 Metric Ton/Week Career Henan Chemical Co Contact Supplier
Methane, chloro-
Cas No: 74-87-3
No Data No Data 1-10 Metric Ton/Month Shandong Hanjiang Chemical Co., Ltd. Contact Supplier

74-87-3 Usage

General Description

A colorless gas with a faint sweet odor. Shipped as a liquid under its vapor pressure. A leak may either be liquid or vapor. Contact with the liquid may cause frostbite by evaporative cooling. Easily ignited. Vapors heavier than air. Can asphyxiate by the displacement of air. Under prolonged exposure to fire or intense heat the containers may rupture violently and rocket. Used to make other chemicals and as a herbicide.

Reactivity Profile

METHYL CHLORIDE can react vigorously with oxidizing agents. May react explosively with sodium, potassium, sodium-potassium alloy, magnesium, zinc. Reacts with aluminum powder in the presence of catalytic amounts of aluminum chloride to form pyrophoric trimethylaluminum. When heated to decomposition, METHYL CHLORIDE emits highly toxic fumes of chlorine [Bretherick, 5th ed., 1995, p. 176].

Purification Methods

Bubble methyl chloride through a sintered-glass disc dipped into conc H2SO4, then wash it with water, condense it at low temperature and fractionally distil it. It has been distilled from AlCl3 at -80o. Alternatively, pass it through towers containing AlCl3, soda-lime and P2O5, then condense and fractionally distil it. Store it as a gas. [Beilstein 1 IV 28.]

Uses

manufacture of silicones, tetramethyleads. Solvent catalyst for butyl rubber. Has been used as a refrigerant.

Health Hazard

Inhalation causes nausea, vomiting, weakness, headache, emotional disturbances; high concentrations cause mental confusion, eye disturbances, muscular tremors, cyanosis, convulsions. Contact of liquid with skin may cause frostbite.

Air & Water Reactions

Highly flammable.

Definition

ChEBI: A one-carbon compound that is methane in which one of the hydrogens is replaced by a chloro group.

Chemical Properties

Methyl chloride,CH3CI, is a flammable, narcotic,colorless compressed gas or liquid with a faintly sweet odor.Slightly soluble in water and soluble in alcohol this gas boils at -23.7℃ and freezes at -97.6℃ and is used as a refrigerant, catalyst carrier, and methylating agent. Also known as chloromethane.
InChI:InChI=1/CH3Cl/c1-2/h1H3

74-87-3 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (295507)  Chloromethane  ≥99.5% 74-87-3 295507-810G-EU 13,419.90CNY Detail
Supelco (48622)  Chloromethanesolution  200 μg/mL in methanol, analytical standard 74-87-3 000000000000048622 207.09CNY Detail
TCI America (M2813)  Methyl Chloride (ca. 5.7% in Tetrahydrofuran, ca. 1mol/L)   74-87-3 100mL 1,250.00CNY Detail

74-87-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Chloromethane

1.2 Other means of identification

Product number -
Other names Methane, chloro-

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Volatile organic compounds
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:74-87-3 SDS

74-87-3Synthetic route

methyl 2,4-dichlorophenoxyacetate
1928-38-7

methyl 2,4-dichlorophenoxyacetate

A

2,4-Dichlorophenoxyacetic acid
94-75-7

2,4-Dichlorophenoxyacetic acid

B

methylene chloride
74-87-3

methylene chloride

Conditions
ConditionsYield
With hydrogenchloride; zinc(II) chloride In water at 140℃; for 4h; Reagent/catalyst; Temperature;A 99.6%
B 98.1%
dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

A

methylphosphonic acid dichloroanhydride
676-97-1

methylphosphonic acid dichloroanhydride

B

methylene chloride
74-87-3

methylene chloride

Conditions
ConditionsYield
With thionyl chloride; N-Formylpiperidine for 19h; Heating; various conditions and cactalasts investigated;A 99.2%
B n/a
methyl o-(N-methylcarbamoyl)phenyl sulphoxide
54705-23-6

methyl o-(N-methylcarbamoyl)phenyl sulphoxide

A

2-methyl-1,2-benzisothiazole-3(2H)-one
2527-66-4

2-methyl-1,2-benzisothiazole-3(2H)-one

B

methylene chloride
74-87-3

methylene chloride

Conditions
ConditionsYield
With thionyl chloride In tetrachloromethane for 5h; Heating;A 99%
B n/a
[PdCl(N,N′-di-metyl-2,11-diaza[3,3](2,6)pyridinophane)(CH3)](2+)

[PdCl(N,N′-di-metyl-2,11-diaza[3,3](2,6)pyridinophane)(CH3)](2+)

tetraethylammonium chloride
56-34-8

tetraethylammonium chloride

A

methylene chloride
74-87-3

methylene chloride

[PdCl2(N,N-di-metyl-2,11-diaza[3,3](2,6)pyridinophane)]
1414791-67-5

[PdCl2(N,N-di-metyl-2,11-diaza[3,3](2,6)pyridinophane)]

Conditions
ConditionsYield
In acetonitrile at 20℃; for 1h; Mechanism; Darkness;A 99%
B 99%
phosgene
75-44-5

phosgene

2,3-bis(dimethylamino)quinol-4-one
104953-88-0

2,3-bis(dimethylamino)quinol-4-one

A

methylene chloride
74-87-3

methylene chloride

B

4-Dimethylamino-3-methyl-3H-oxazolo[4,5-c]quinolin-2-one
104953-90-4

4-Dimethylamino-3-methyl-3H-oxazolo[4,5-c]quinolin-2-one

Conditions
ConditionsYield
With triethylamine In dichloromethane for 3h; Product distribution; Ambient temperature; aminoquinolones with COCl2;A n/a
B 98%
With triethylamine In dichloromethane for 3h; Ambient temperature;A n/a
B 98%
N-phenyl-2-(methylsulfinyl)benzamide
79054-68-5

N-phenyl-2-(methylsulfinyl)benzamide

A

2-phenyl-1,2-benzisothiazolin-3-one
2527-03-9

2-phenyl-1,2-benzisothiazolin-3-one

B

methylene chloride
74-87-3

methylene chloride

Conditions
ConditionsYield
With thionyl chloride In dichloromethane for 0.166667h; Heating;A 98%
B n/a
N-Cyclohexyl-2-methanesulfinyl-benzamide
79054-66-3

N-Cyclohexyl-2-methanesulfinyl-benzamide

A

methylene chloride
74-87-3

methylene chloride

B

2-cyclohexyl-1,2-benzisothiazol-3(2H)-one
2527-02-8

2-cyclohexyl-1,2-benzisothiazol-3(2H)-one

Conditions
ConditionsYield
With thionyl chloride In dichloromethane Heating;A n/a
B 98%
2-Methanesulfinyl-N-p-tolyl-benzamide
79054-69-6

2-Methanesulfinyl-N-p-tolyl-benzamide

A

methylene chloride
74-87-3

methylene chloride

B

2-(4-tolyl)-1,2-benzisothiazol-3-one
2514-30-9

2-(4-tolyl)-1,2-benzisothiazol-3-one

Conditions
ConditionsYield
With thionyl chloride In dichloromethane Heating;A n/a
B 98%
N-Benzyl-2-methanesulfinyl-benzamide
79054-67-4

N-Benzyl-2-methanesulfinyl-benzamide

A

methylene chloride
74-87-3

methylene chloride

B

2-benzylbenzo[d]isothiazol-3(2H)-one
2514-36-5

2-benzylbenzo[d]isothiazol-3(2H)-one

Conditions
ConditionsYield
With thionyl chloride In dichloromethane Heating;A n/a
B 98%
N-Isopropyl-2-methanesulfinyl-benzamide
79054-64-1

N-Isopropyl-2-methanesulfinyl-benzamide

A

methylene chloride
74-87-3

methylene chloride

B

2-isopropyl-1,2-benzisothiazolin-3-one

2-isopropyl-1,2-benzisothiazolin-3-one

Conditions
ConditionsYield
With thionyl chloride In dichloromethane Heating;A n/a
B 97%
Cp(CO)2Re(CH3)2

Cp(CO)2Re(CH3)2

A

tricarbonylcyclopentadienylrhenium

tricarbonylcyclopentadienylrhenium

B

methylene chloride
74-87-3

methylene chloride

C

C5H5Re(CO)2(CH3)Cl

C5H5Re(CO)2(CH3)Cl

D

acetyl chloride
75-36-5

acetyl chloride

E

acetone
67-64-1

acetone

Conditions
ConditionsYield
With tetrachloromethane; carbon monoxide In tetrachloromethane Irradiation (UV/VIS); Irradiation of complex at 350-380 nm under 20 atm of CO in CCl4;;A 97%
B 19%
C <4
D 152 %
E 6%
dichloromethane
75-09-2

dichloromethane

A

methylene chloride
74-87-3

methylene chloride

B

Difluoromethane
75-10-5

Difluoromethane

C

R32
593-70-4

R32

D

trifluoromethan
75-46-7

trifluoromethan

Conditions
ConditionsYield
With hydrogen fluoride; antimony(III) fluoride; antimony pentafluoride at 5 - 100℃; under 12504.7 Torr;A n/a
B 96.9%
C 3.08%
D n/a
antimony pentafluorideA n/a
B 96.4%
C 3.56%
D n/a
N-Ethyl-2-methanesulfinyl-benzamide
79054-63-0

N-Ethyl-2-methanesulfinyl-benzamide

A

2-Ethylbenzisothiazolin-3-on
4299-06-3

2-Ethylbenzisothiazolin-3-on

B

methylene chloride
74-87-3

methylene chloride

Conditions
ConditionsYield
With thionyl chloride In dichloromethane Heating;A 96%
B n/a
1-chloro-2,2,6,6-tetramethylpiperidine
32579-76-3

1-chloro-2,2,6,6-tetramethylpiperidine

A

methylene chloride
74-87-3

methylene chloride

B

2,2,6-trimethyl-2,3,4,5-tetrahydropyridine
112269-97-3

2,2,6-trimethyl-2,3,4,5-tetrahydropyridine

Conditions
ConditionsYield
With 2,2'-azobis(isobutyronitrile) In trifluoroacetic acid at 80℃;A 95%
B 8.5 g
2,4-dinitrobenzenesulfenyl chloride
528-76-7

2,4-dinitrobenzenesulfenyl chloride

A

methylene chloride
74-87-3

methylene chloride

B

bis(2,4-dinitrophenyl) disulphide
2217-55-2

bis(2,4-dinitrophenyl) disulphide

C

methyl 2,4-dinitriophenyl sulfide
2363-23-7

methyl 2,4-dinitriophenyl sulfide

Conditions
ConditionsYield
With tetramethylstannane; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 25℃; for 4h; Mechanism; other sulfenyl halides, other reagents: tetraethylstannane, hexamethyldistannane, tributylvinylstannane, tetracyclohexylstannane, tetraphenylstannane, cyclohexene, tetramethylgermane, other solvent: THF-d8;A n/a
B 95%
C n/a
aluminium trichloride
7446-70-0

aluminium trichloride

methoxybenzene
100-66-3

methoxybenzene

A

methylene chloride
74-87-3

methylene chloride

B

dichloroaluminium phenoxide

dichloroaluminium phenoxide

Conditions
ConditionsYield
In neat (no solvent) 1:1 mixt. was heated at 130°C for 6 h;A 95%
B n/a
{PdCl[Ind(Ph2P=S)2]}(nBu4N)

{PdCl[Ind(Ph2P=S)2]}(nBu4N)

methyl iodide
74-88-4

methyl iodide

A

methylene chloride
74-87-3

methylene chloride

{PdI[Ind(Me)(Ph2P=S)2]}

{PdI[Ind(Me)(Ph2P=S)2]}

C

tetra-(n-butyl)ammonium iodide
311-28-4

tetra-(n-butyl)ammonium iodide

Conditions
ConditionsYield
In dichloromethane at 40℃; for 24h; Inert atmosphere;A n/a
B 95%
C n/a
methyl dichlorophosphite
3279-26-3

methyl dichlorophosphite

trifluoromethaneselenenyl chloride
1495-26-7

trifluoromethaneselenenyl chloride

A

methylene chloride
74-87-3

methylene chloride

B

Se-trifluoromethylphosphorodichloridoselenoate
77001-46-8

Se-trifluoromethylphosphorodichloridoselenoate

Conditions
ConditionsYield
With antimonypentachloride at -10 - 5℃;A n/a
B 94%
pyridine
110-86-1

pyridine

C6H12Cl2O2Pt

C6H12Cl2O2Pt

A

methylene chloride
74-87-3

methylene chloride

B

cis-Cl(py)Pt(COMe)[C(OMe)(Me)]
1395411-03-6

cis-Cl(py)Pt(COMe)[C(OMe)(Me)]

Conditions
ConditionsYield
In tetrahydrofuran-d8 at 55℃; for 2h;A n/a
B 93%
methanol
67-56-1

methanol

1-(1-naphthyl)-3-phenyl-2,2-dichloroaziridine
31528-95-7

1-(1-naphthyl)-3-phenyl-2,2-dichloroaziridine

A

methylene chloride
74-87-3

methylene chloride

B

Dimethyl ether
115-10-6

Dimethyl ether

C

methyl 2-chloro-2-phenylethanoate
7476-66-6

methyl 2-chloro-2-phenylethanoate

D

methyl 2-methoxy-2-phenylacetate
3558-61-0

methyl 2-methoxy-2-phenylacetate

E

1-naphthylamine hydrochloride
552-46-5

1-naphthylamine hydrochloride

Conditions
ConditionsYield
Product distribution; Heating;A n/a
B n/a
C n/a
D n/a
E 91%
C6H12Cl2O2Pt

C6H12Cl2O2Pt

tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

A

methylene chloride
74-87-3

methylene chloride

B

(n-Bu4NCl)[Cl2Pt(COMe)(C(OMe)(Me))]
1395411-09-2

(n-Bu4NCl)[Cl2Pt(COMe)(C(OMe)(Me))]

Conditions
ConditionsYield
In dichloromethane-d2 at 20℃; for 0.25h;A n/a
B 87%
phosgene
75-44-5

phosgene

2,3-Bis-dimethylamino-1H-benzo[h]quinolin-4-one
104953-89-1

2,3-Bis-dimethylamino-1H-benzo[h]quinolin-4-one

A

methylene chloride
74-87-3

methylene chloride

B

12-Dimethylamino-17-methyl-17H-15-oxa-11,17-diaza-cyclopenta[a]phenanthren-16-one
104953-91-5

12-Dimethylamino-17-methyl-17H-15-oxa-11,17-diaza-cyclopenta[a]phenanthren-16-one

Conditions
ConditionsYield
With triethylamine In dichloromethane for 3h; Ambient temperature;A n/a
B 85%
2,2,2-trichloro-N-methylacetimidoyl chloride
57182-16-8

2,2,2-trichloro-N-methylacetimidoyl chloride

phosphorous acid trimethyl ester
121-45-9

phosphorous acid trimethyl ester

A

C7H15Cl2NO6P2
70795-51-6

C7H15Cl2NO6P2

B

methylene chloride
74-87-3

methylene chloride

Conditions
ConditionsYield
In toluene for 2h; Heating;A 84%
B n/a
N-methyl-N-(methoxymethyl)-aniline
13657-45-9

N-methyl-N-(methoxymethyl)-aniline

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

A

methylene chloride
74-87-3

methylene chloride

B

<(methylphenylamino)methyl>diphenylphosphine oxide
76527-75-8

<(methylphenylamino)methyl>diphenylphosphine oxide

Conditions
ConditionsYield
In tetrahydrofuranA n/a
B 83%
N-ethyl-2,2,2-trichloro-acetimidoyl chloride
57182-25-9

N-ethyl-2,2,2-trichloro-acetimidoyl chloride

phosphorous acid trimethyl ester
121-45-9

phosphorous acid trimethyl ester

A

methylene chloride
74-87-3

methylene chloride

B

{2,2-Dichloro-1-[(dimethoxy-phosphoryl)-ethyl-amino]-vinyl}-phosphonic acid dimethyl ester
70795-55-0

{2,2-Dichloro-1-[(dimethoxy-phosphoryl)-ethyl-amino]-vinyl}-phosphonic acid dimethyl ester

Conditions
ConditionsYield
In toluene for 2h; Heating;A n/a
B 82%
3-chlorobenzotrichloride
2136-81-4

3-chlorobenzotrichloride

dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

A

methylene chloride
74-87-3

methylene chloride

B

methyl 3-chlorobenzoate
2905-65-9

methyl 3-chlorobenzoate

C

methylphosphonic acid anhydride

methylphosphonic acid anhydride

Conditions
ConditionsYield
at 180℃; for 53h;A n/a
B 81%
C n/a
Dichlorodiphenylmethane
2051-90-3

Dichlorodiphenylmethane

dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

A

benzophenone
119-61-9

benzophenone

B

methylene chloride
74-87-3

methylene chloride

C

methylphosphonic acid anhydride

methylphosphonic acid anhydride

Conditions
ConditionsYield
at 100 - 120℃; for 28h;A 80%
B n/a
C 51%
benzylidene dichloride
98-87-3

benzylidene dichloride

Methyl Diisopropylphosphinate
18632-46-7

Methyl Diisopropylphosphinate

A

methylene chloride
74-87-3

methylene chloride

B

diisopropylphosphoryl chloride
1112-15-8

diisopropylphosphoryl chloride

C

benzaldehyde
100-52-7

benzaldehyde

D

diisopropylphosphinic anhydride
67949-89-7

diisopropylphosphinic anhydride

Conditions
ConditionsYield
at 180℃; for 17h; Product distribution; Mechanism; other gem-dihalide: benzal bromide, other methyl esters of tetracoordinated phosphorus acids, various reactants ratio, other reaction temperature and time;A n/a
B n/a
C 79.7%
D 75%
4-chlorotrichloromethylbenzene
5216-25-1

4-chlorotrichloromethylbenzene

dimethyl methane phosphonate
756-79-6

dimethyl methane phosphonate

A

Methyl 4-chlorobenzoate
1126-46-1

Methyl 4-chlorobenzoate

B

methylene chloride
74-87-3

methylene chloride

C

methylphosphonic acid anhydride

methylphosphonic acid anhydride

Conditions
ConditionsYield
at 180℃; for 53h;A 79%
B n/a
C n/a
N-t-butyl-2-(methylsulphinyl)benzamide
79054-65-2

N-t-butyl-2-(methylsulphinyl)benzamide

A

methylene chloride
74-87-3

methylene chloride

B

2-(tert-butyl)benzo[d]isothiazol-3(2H)-one
35159-95-6

2-(tert-butyl)benzo[d]isothiazol-3(2H)-one

Conditions
ConditionsYield
With thionyl chloride In dichloromethane for 1h; Ambient temperature;A n/a
B 77%
With thionyl chloride In dichloromethane Heating;A n/a
B 77%
C18H42FSi3(1-)*Li(1+)

C18H42FSi3(1-)*Li(1+)

methylene chloride
74-87-3

methylene chloride

1,1,3,3-tetra-tert-butyl-2-fluoro-1,2,3-trimethyl-trisilane

1,1,3,3-tetra-tert-butyl-2-fluoro-1,2,3-trimethyl-trisilane

Conditions
ConditionsYield
In tetrahydrofuran; hexane at 20℃;100%
methylene chloride
74-87-3

methylene chloride

N,N’-bis[3-(dimethylamino)propyl]-1,4,5,8-naphthalenetetracarboxylic 1,8:4,5-diimide
3436-54-2

N,N’-bis[3-(dimethylamino)propyl]-1,4,5,8-naphthalenetetracarboxylic 1,8:4,5-diimide

hexa-N-methyl-N,N'-[3,3'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydro-benzo[lmn][3,8]phenanthroline-2,7-diyl)-dipropyl]-bis-ammonium
83356-30-3

hexa-N-methyl-N,N'-[3,3'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydro-benzo[lmn][3,8]phenanthroline-2,7-diyl)-dipropyl]-bis-ammonium

Conditions
ConditionsYield
In chloroform at 20℃; for 24h; Green chemistry;100%
methylene chloride
74-87-3

methylene chloride

2-(2-methoxyethoxy)ethyl alcohol
111-77-3

2-(2-methoxyethoxy)ethyl alcohol

1,2-dimethoxyethane
110-71-4

1,2-dimethoxyethane

Conditions
ConditionsYield
With sodium hydroxide In water at 60℃;99.8%
methylene chloride
74-87-3

methylene chloride

dimethyltin dichloride
753-73-1

dimethyltin dichloride

trimethylsulfonium chloride
3086-29-1

trimethylsulfonium chloride

methyltin(IV) trichloride
993-16-8

methyltin(IV) trichloride

Conditions
ConditionsYield
tin(IV) chloride99.7%
methylene chloride
74-87-3

methylene chloride

3-(2-chloro-5-(2,6-dioxo-4-trifluoromethyl-3,6-dihydropyrimidine-1(2H)-yl)-4-fluorophenyl)-5-methyl-4,5-dihydroisoxazole-5-carboxylic acid methyl ester

3-(2-chloro-5-(2,6-dioxo-4-trifluoromethyl-3,6-dihydropyrimidine-1(2H)-yl)-4-fluorophenyl)-5-methyl-4,5-dihydroisoxazole-5-carboxylic acid methyl ester

C18H14ClF4N3O5

C18H14ClF4N3O5

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; sodium carbonate In ethyl acetate at 95 - 105℃; under 6750.68 Torr; for 11h; Autoclave;99.2%
methylene chloride
74-87-3

methylene chloride

benzyl α-(N,N-dimethylamino)ethyl Boc-glutamate
103897-73-0

benzyl α-(N,N-dimethylamino)ethyl Boc-glutamate

α-(γ-benzyloxy-Boc-glutamyl)choline chloride
103897-79-6

α-(γ-benzyloxy-Boc-glutamyl)choline chloride

Conditions
ConditionsYield
In ethyl acetate; benzene for 168h; Ambient temperature;99%
methylene chloride
74-87-3

methylene chloride

α-tert-butyl γ-(N,N-dimethylamino)ethyl Z-glutamate
101463-49-4

α-tert-butyl γ-(N,N-dimethylamino)ethyl Z-glutamate

γ-(α-tert-butyloxy-Z-glutamyl)choline chloride
101463-50-7

γ-(α-tert-butyloxy-Z-glutamyl)choline chloride

Conditions
ConditionsYield
In ethyl acetate; benzene for 168h; Ambient temperature;99%
Tri-n-octylamine
1116-76-3

Tri-n-octylamine

methylene chloride
74-87-3

methylene chloride

phenylacetonitrile
140-29-4

phenylacetonitrile

2,3-dimethylphenylacetonitrile
76574-43-1

2,3-dimethylphenylacetonitrile

Conditions
ConditionsYield
With sodium hydroxide In water99%
[(κ2-P,N)-2-(N,N-dimethylamino)ethyldiphenylphosphino]dimethylplatinum(II)
240123-21-1

[(κ2-P,N)-2-(N,N-dimethylamino)ethyldiphenylphosphino]dimethylplatinum(II)

methylene chloride
74-87-3

methylene chloride

[(κ(2)-P,N)-Ph2PCH2CH2NMe2]PtMe3Cl

[(κ(2)-P,N)-Ph2PCH2CH2NMe2]PtMe3Cl

Conditions
ConditionsYield
In benzene-d6 all manipulations under Ar atm.; MeCl bubbled through soln. of Pt compd., then heated to .60°C for 24 h; crystd. from benzene, elem. anal.;99%
In benzene-d6 all manipulations under Ar atm.; MeCl bubbled through soln. of Pt compd., then heated to .60°C for 12 h; crystd. from benzene, elem. anal.;95%
[(κ(2)-P,N)-Me2NCH2CH2PPh2]Pt(CD3)2
484065-57-8

[(κ(2)-P,N)-Me2NCH2CH2PPh2]Pt(CD3)2

methylene chloride
74-87-3

methylene chloride

[(κ(2)-P,N)-Ph2PCH2CH2NMe2]PtMe(CD3)3Cl
484065-61-4

[(κ(2)-P,N)-Ph2PCH2CH2NMe2]PtMe(CD3)3Cl

Conditions
ConditionsYield
In benzene-d6 all manipulations under Ar atm.; MeCl bubbled through soln. of Pt compd., then heated to .60°C for 24 h;99%
teflic acid
57458-27-2

teflic acid

methylene chloride
74-87-3

methylene chloride

triethylaluminum
97-93-8

triethylaluminum

AlF20O4Te4(1-)*C2H6Cl(1+)

AlF20O4Te4(1-)*C2H6Cl(1+)

Conditions
ConditionsYield
at -40℃; Schlenk technique; Glovebox; Inert atmosphere;99%
methylene chloride
74-87-3

methylene chloride

1,3-bis(dimethylamino)isopropyl methacrylate
21476-57-3

1,3-bis(dimethylamino)isopropyl methacrylate

1,3-bis(trimethylammonium)-2-propyl methacrylate chloride

1,3-bis(trimethylammonium)-2-propyl methacrylate chloride

Conditions
ConditionsYield
In acetonitrile at 73℃; under 1500.15 Torr; for 24h; Conversion of starting material;98.6%
In acetonitrile at 71℃; under 1500.15 Torr; for 23h; Conversion of starting material;96%
In acetonitrile at 80 - 85℃; under 1500.15 Torr; for 23 - 28h; Product distribution / selectivity;93.1%
In acetonitrile at 72℃; under 1500.15 Torr; for 23h; Product distribution / selectivity;90.2%
In acetone at 50 - 80℃; under 1500.15 Torr; for 22 - 25h; Product distribution / selectivity;53.8%
methylene chloride
74-87-3

methylene chloride

sodium thiophenolate
930-69-8

sodium thiophenolate

methyl-phenyl-thioether
100-68-5

methyl-phenyl-thioether

Conditions
ConditionsYield
at 160℃; under 66756.7 Torr; for 5h; Temperature; Pressure; Concentration; Autoclave; Inert atmosphere;98.6%
17α-cyano-17β-hydroxyandrost-1,4-dien-3-one

17α-cyano-17β-hydroxyandrost-1,4-dien-3-one

methylene chloride
74-87-3

methylene chloride

17α-Hydroxypregna-1,4-diene-3,20-dione
2477-61-4

17α-Hydroxypregna-1,4-diene-3,20-dione

Conditions
ConditionsYield
Stage #1: methylene chloride With magnesium In tetrahydrofuran at 30 - 35℃;
Stage #2: 17α-cyano-17β-hydroxyandrost-1,4-dien-3-one In tetrahydrofuran at 50 - 55℃;
98.6%
Stage #1: methylene chloride With magnesium In tetrahydrofuran at 35 - 98℃;
Stage #2: 17α-cyano-17β-hydroxyandrost-1,4-dien-3-one In tetrahydrofuran at 50 - 55℃;
92.5%
methylene chloride
74-87-3

methylene chloride

N-hydroxy-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenylcarbamic acid methyl ester

N-hydroxy-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenylcarbamic acid methyl ester

pyraclostrobin
175013-18-0

pyraclostrobin

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In acetone at 30 - 50℃; under 2250.23 - 3750.38 Torr; Reagent/catalyst; Solvent;98.5%
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydrogencarbonate In water; toluene Reagent/catalyst; Solvent; Autoclave; Alkaline conditions;96.2%
With nano zinc ferrite In dichloromethane at 120℃; under 3000.3 - 4350.44 Torr; for 4h; Autoclave;82.4%
methylene chloride
74-87-3

methylene chloride

methylthiol
74-93-1

methylthiol

Conditions
ConditionsYield
With hydrogen sulfide at 260 - 800℃; under 6000.6 Torr; for 0.216667h; Temperature; Pressure; Inert atmosphere; Calcination;98.4%
With hydrosulfide anion In gas Rate constant; Thermodynamic data; reaction efficiency, ΔH0Rx;
With sodium hydrogensulfide; water unter Druck;
methylene chloride
74-87-3

methylene chloride

1-amino-9,10-anthracenedione
82-45-1

1-amino-9,10-anthracenedione

1-(methylamino)anthraquinone
82-38-2

1-(methylamino)anthraquinone

Conditions
ConditionsYield
With ammonium nitrate In aq. phosphate buffer at 50℃; for 5h; Reagent/catalyst; Solvent;98.2%
1,4-diaza-bicyclo[2.2.2]octane
280-57-9

1,4-diaza-bicyclo[2.2.2]octane

methylene chloride
74-87-3

methylene chloride

1-Methyl-4-aza-1-azoniabicyclo<2.2.2>octane tetrafluoroborate

1-Methyl-4-aza-1-azoniabicyclo<2.2.2>octane tetrafluoroborate

Conditions
ConditionsYield
With sodium tetrafluoroborate In acetonitrile at 20℃;98%
With sodium tetrafluoroborate In acetonitrile Ambient temperature; sealed tube;97%
methylene chloride
74-87-3

methylene chloride

(R)-(-)-9-hydroxydecanoic acid
35433-73-9

(R)-(-)-9-hydroxydecanoic acid

(-)-(R)-9-Hydroxydecansaeure-methylester
85551-52-6

(-)-(R)-9-Hydroxydecansaeure-methylester

Conditions
ConditionsYield
98%
1,4-diaza-bicyclo[2.2.2]octane
280-57-9

1,4-diaza-bicyclo[2.2.2]octane

methylene chloride
74-87-3

methylene chloride

potassium trifluoromethansulfonate
2926-27-4

potassium trifluoromethansulfonate

1-methyl-4-aza-1-azoniabicyclo[2.2.2]octane trifluoromethanesulfonate
140681-58-9

1-methyl-4-aza-1-azoniabicyclo[2.2.2]octane trifluoromethanesulfonate

Conditions
ConditionsYield
In acetonitrile Ambient temperature; sealed tube;98%
methylene chloride
74-87-3

methylene chloride

diafenthiuron
80060-09-9

diafenthiuron

1-tert-butyl-3-(2,6-diisopropyl-4-phenoxyphenyl)-2-methylisothiourea

1-tert-butyl-3-(2,6-diisopropyl-4-phenoxyphenyl)-2-methylisothiourea

Conditions
ConditionsYield
With potassium hydroxide In butanone at 70℃; for 4h; Autoclave;98%

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