(S)-tert-butyl isoxazolidine-3-carboxylate

Base Information

Chemical Name:(S)-tert-butyl isoxazolidine-3-carboxylate
CAS No.:78266-75-8
Molecular Formula:C₈H₁₅NO₃
Molecular Weight:173.212
Hs Code.:

Synonyms:(S)-tert-butyl isoxazolidine-3-carboxylate

Suppliers and Price of (S)-tert-butyl isoxazolidine-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-tert-butyl isoxazolidine-3-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S)-tert-butyl isoxazolidine-3-carboxylate

There total 1 articles about (S)-tert-butyl isoxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7633-32-1
tert-butyl glyoxylate

: 78266-75-8
(S)-tert-butyl isoxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / 17 h / 80 °C / 30003 Torr / Autoclave

2: perchloric acid / acetonitrile; water

With perchloric acid; In chloroform; water; acetonitrile;
DOI:10.1002/anie.201204144 DOI:10.1002/anie.201204144

Reference yield: 84.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 78266-75-8
(S)-tert-butyl isoxazolidine-3-carboxylate

: 78266-76-9
t-butyl (S)-2-benzyloxycarbonyl-3-isoxazolidinecarboxylate

Guidance literature:: With sodium hydrogencarbonate; sodium carbonate; In chloroform; for 8.5h; Ambient temperature;
DOI:10.1002/hlca.19830660424

Reference yield:

: 78266-75-8
(S)-tert-butyl isoxazolidine-3-carboxylate

: 47307-26-6,149967-07-7
(S)-2-benzyloxycarbonylamino-succinic acid 1-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.75 g / hydrogen / 5percent Rh/C / ethanol / 20 h / Ambient temperature

2: 79 percent / 1 M NaHCO₃, 1 M Na₂CO₃ / CHCl₃ / 5 h / Ambient temperature

3: 84 percent / KMnO₄ / acetone; acetic acid / 3.5 h / Ambient temperature

With potassium permanganate; hydrogen; sodium hydrogencarbonate; sodium carbonate; Rh on carbon; In ethanol; chloroform; acetic acid; acetone;
DOI:10.1002/hlca.19830660424