Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Base Information

Chemical Name:Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid
CAS No.:75810-03-6
Molecular Formula:C₂₃H₃₂O₉
Molecular Weight:452.502
Hs Code.:

Synonyms:Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid

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Chemical Property of Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid

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Technology Process of Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid

There total 4 articles about Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 75810-02-5
Methyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-D-mannopyranosyl)-4-O-benzoyl-6-brom-2,6-didesoxy-α-D-arabino-hexopyranosid

: 75810-03-6
Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Guidance literature:: With polyhydrogenmethylsiloxane; bis(tri-n-butyltin)oxide; In toluene; at 100 ℃; for 0.5h;

Reference yield:

: 70717-91-8,78086-68-7
Methyl-3-O-(4-O-acetyl-2,6-didesoxy-2-iod-3-C-methyl-α-D-mannopyranosyl)-4,6-O-benzyliden-2-desoxy-α-D-arabino-hexopyranosid

: 75810-03-6
Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / N-bromosuccinimide, BaCO₃ / CCl₄ / 0.25 h / Heating

2: 58 percent / bis(tri-n-butyltin) oxide, polyhydrogenmethylsiloxane / toluene / 0.5 h / 100 °C

With N-Bromosuccinimide; polyhydrogenmethylsiloxane; barium carbonate; bis(tri-n-butyltin)oxide; In tetrachloromethane; toluene;

Reference yield:

: 78086-64-3
4-O-Acetyl-1,5-anhydro-2,6-didesoxy-3-C-methyl-D-arabino-hex-1-enit

: 75810-03-6
Methyl-3-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-arabinohexopyranosyl)-4-O-benzoyl-2,6-didesoxy-α-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / N-iodosuccinimide / acetonitrile / 5 °C

2: 63 percent / N-bromosuccinimide, BaCO₃ / CCl₄ / 0.25 h / Heating

3: 58 percent / bis(tri-n-butyltin) oxide, polyhydrogenmethylsiloxane / toluene / 0.5 h / 100 °C

With N-Bromosuccinimide; N-iodo-succinimide; polyhydrogenmethylsiloxane; barium carbonate; bis(tri-n-butyltin)oxide; In tetrachloromethane; toluene; acetonitrile;